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Chemical Structure| 141483-49-0 Chemical Structure| 141483-49-0

Structure of 141483-49-0

Chemical Structure| 141483-49-0

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Product Details of [ 141483-49-0 ]

CAS No. :141483-49-0
Formula : C23H23NO2
M.W : 345.43
SMILES Code : O=C(OCC1=CC=CC=C1)CN(CC2=CC=CC=C2)CC3=CC=CC=C3
MDL No. :MFCD00193075

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Application In Synthesis of [ 141483-49-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 141483-49-0 ]

[ 141483-49-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 141483-49-0 ]
  • [ 101-06-4 ]
YieldReaction ConditionsOperation in experiment
With lithium aluminium tetrahydride; In diethyl ether; at 0℃;Inert atmosphere; General procedure: Benzyl 2-(dibenzylamino) derivatives (3.92 mmol, 1 equiv.) were added to a stirred suspension of lithium aluminum hydride (11.75 mmol, 3 equiv.) in Et2O (15 ml) under argon atmosphere at 0 C. After 15 min cooling bath was removed and mixtures were stirred overnight and cooled again to 0 C. Mixtures has been worked-up by careful dropwise addition of 0.5 mL of H2O, 1 mL of 15% KOH and 1.5 mL of H2O. Aluminum salts were removed by filtration, and the filtrates were concentrated under reduced pressure. Crude products were purified by flash chromatography (hexane/ethyl acetate 70:30, v/v).
 

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