Home Cart Sign in  
Chemical Structure| 1428881-71-3 Chemical Structure| 1428881-71-3

Structure of 1428881-71-3

Chemical Structure| 1428881-71-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1428881-71-3 ]

CAS No. :1428881-71-3
Formula : C7H5IN4
M.W : 272.05
SMILES Code : IC1=CN=CN=C1N2C=CN=C2

Safety of [ 1428881-71-3 ]

Application In Synthesis of [ 1428881-71-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1428881-71-3 ]

[ 1428881-71-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 288-32-4 ]
  • [ 63558-65-6 ]
  • [ 1428881-71-3 ]
YieldReaction ConditionsOperation in experiment
52.1% Preparation 60A: 4-(lH-Imidazol-l- l)-5-iodopyrimidine[00248] To a solution of lH-imidazole (0.085 g, 1.248 mmol) in THF (Volume: 10 mL) was added sodium hydride (0.062 g, 1.560 mmol). After 15 minutes at room temperature, <strong>[63558-65-6]4-chloro-5-iodopyrimidine</strong> (0.25 g, 1.040 mmol) was added as a solution in THF (5 mL). After 2 h at room temperature, the reaction was quenched with water. The reaction mixture was extracted with EtOAc (3X). The combined organics were dried over MgS04, filtered and concentrated to give the title compound (0.155 g, 0.541 mmol, 52.1% yield) as a pale yellow solid. ESI MS (M+H)+ = 273.0.
 

Historical Records

Technical Information

Categories