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Chemical Structure| 14422-49-2 Chemical Structure| 14422-49-2

Structure of 14422-49-2

Chemical Structure| 14422-49-2

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Product Details of [ 14422-49-2 ]

CAS No. :14422-49-2
Formula : C9H8ClNO3
M.W : 213.62
SMILES Code : O=C(O)C1=CC=CC=C1NC(CCl)=O
MDL No. :MFCD00029924

Safety of [ 14422-49-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H315-H318-H335
Precautionary Statements:P261-P264-P270-P271-P280-P302+P352-P304+P340-P305+P351+P338-P310-P330-P332+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 14422-49-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14422-49-2 ]

[ 14422-49-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 13920-91-7 ]
  • [ 14422-49-2 ]
  • C17H15ClN2OS [ No CAS ]
YieldReaction ConditionsOperation in experiment
With trichlorophosphate; In acetonitrile; at 150℃; for 0.25h;Microwave irradiation; General procedure: To a solution of anthranilic acid 2 (0.40 mmol) and Huenig's base (0.60 mmol) in anhydrous acetonitrile (1.0 mL) was added a solution of chloroacetyl chloride (0.44 mmol) in acetonitrile (0.5 mL) at 4 C. After stirring at r.t. for 2 h, POCl3 (112 muL, 1.2 mmol, 3.0 equiv) was added followed by a solution of aniline (0.60 mmol) in acetonitrile (0.50 mL). The reaction mixture was heated in a microwave reactor at 150 C for 15 min, cooled to r.t. and treated with K2CO3 (300 mg) and EtOH (1.0 mL). The mixture was heated at 150 C for 5 min in the microwave reactor. To this mixture, a solution of piperazine, morpholine, or piperidine (0.44 mmol) in EtOH (0.5 mL) was added. The mixture was heated in the microwave reactor for 10 min at 150 C and filtered. The filtrate was concentrated under reduced pressure and the residue was purified by preparative HPLC.
  • 2
  • [ 1019442-22-8 ]
  • [ 14422-49-2 ]
  • C18H16BrClN2O2 [ No CAS ]
 

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