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Chemical Structure| 14469-83-1 Chemical Structure| 14469-83-1

Structure of 14469-83-1

Chemical Structure| 14469-83-1

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Product Details of [ 14469-83-1 ]

CAS No. :14469-83-1
Formula : C11H15Br
M.W : 227.14
SMILES Code : BrCCCCCC1=CC=CC=C1
MDL No. :MFCD01075177
InChI Key :QICUPOFVENZWSC-UHFFFAOYSA-N
Pubchem ID :285561

Safety of [ 14469-83-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P301+P312-P302+P352-P304+P340-P305+P351+P338

Application In Synthesis of [ 14469-83-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 14469-83-1 ]

[ 14469-83-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 14469-83-1 ]
  • [ 5847-59-6 ]
  • [ 1378872-59-3 ]
YieldReaction ConditionsOperation in experiment
56% With potassium carbonate; In N,N-dimethyl-formamide; at 100℃; for 18h; 2-bromo-4-nitro-1-((5-phenylpentyl)oxy)benzene A mixture of <strong>[5847-59-6]2-bromo-4-nitrophenol</strong> (CAS 5847-59-6) (2.05 g, 9.4 mmol), (5-bromopentyl)benzene (CAS 14469-83-1) (2.41 g, 10.6 mmol) and K2CO3 (3.5 g, 19.1 mmol) was dissolved in DMF (20 mL). The reaction mixture was heated at 100 C. for ~18 h. The mixture was diluted with hexanes:EtOAc (1:1) (~200 mL) and washed with H2O (3*). The organic solution was dried over MgSO4, filtered, and concentrated onto silica gel under vacuum. Auto-column (9.5 hexanes: 0.5 EtOAc) gave Intermediate 1 as a white solid 1.91 g (56%).
 

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