Home Cart Sign in  
HazMat Fee +

There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 1462-33-5 Chemical Structure| 1462-33-5

Structure of 1462-33-5

Chemical Structure| 1462-33-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1462-33-5 ]

CAS No. :1462-33-5
Formula : C3H6Cl2O
M.W : 128.99
SMILES Code : ClCOCCCl
MDL No. :MFCD00191406

Safety of [ 1462-33-5 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225-H300+H310+H330-H314
Precautionary Statements:P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P370+P378
Class:6.1(3)
UN#:2929
Packing Group:

Application In Synthesis of [ 1462-33-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1462-33-5 ]

[ 1462-33-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 161609-84-3 ]
  • [ 1462-33-5 ]
  • [ 959689-78-2 ]
YieldReaction ConditionsOperation in experiment
86% With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20℃; for 5h; Benzyl 4-((2-chloroethoxy)methyl)-4-cyanopiperidine-1-carboxylate. A solution of <strong>[161609-84-3]benzyl 4-cyanopiperidine-1-carboxylate</strong> (10.0 g, 410 mmol) and 2-chloroethyl chloromethyl ether (6.3 mL, 49.2 mmol) in THF (80 mL) was cooled to -78 C. To this solution was added drop wise LiHMDS (50 mL, 50 mmol, 1N in THF) and the resulting mixture was gradually warmed to room temp over 5 h. The reaction was quenched with water and the organic phase was washed with brine, dried (Na2SO4) and concentrated. The residue was purified by flash chromatography (1:1 EtOAc/hexane) to give the title compound as yellow oil (11.9 g, 86% yield). 1H NMR (300 MHz, CDCl3) delta: 7.33-7.31 (5H, m), 5.10 (2H, d, J=5.9 Hz), 4.21 (2H, bs), 3.79-3.76 (2H, m), 3.63-3.60 (2H, m), 3.52-3.51 (2H, m), 3.09 (2H, bs), 1.96-1.92 (2H, m), 1.55-1.51 (2H, m).
 

Historical Records

Technical Information

Categories