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Chemical Structure| 150018-99-8 Chemical Structure| 150018-99-8

Structure of 150018-99-8

Chemical Structure| 150018-99-8

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Product Details of [ 150018-99-8 ]

CAS No. :150018-99-8
Formula : C13H16N2O
M.W : 216.28
SMILES Code : N#CC1(O)CN(CC2=CC=CC=C2)CCC1
MDL No. :MFCD11110454

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Application In Synthesis of [ 150018-99-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 150018-99-8 ]

[ 150018-99-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 773837-37-9 ]
  • [ 50606-58-1 ]
  • [ 150018-99-8 ]
YieldReaction ConditionsOperation in experiment
10.35 g With sodium hydrogensulfite; In tetrahydrofuran; water; at 0℃; for 1.5h; To a stirred solution of 10,0 g (44 mmol) of l-benzyl-3-piperidone hydrochloride hydrate and 3.28 g (66.9 mmol) of sodium cyanide in mixture of 28 ml of tetrahydrofurane and 56 mL of water 17.1 mL of 40 % sodium hydrogen sulfite in 46 ml of water was added dropwise at 0 C. The reaction mixture was stirred at this temperature for 1.5 h. The reaction mixture was extracted with dichloromethane, the combined organic layer was washed with water, dried over anhydrous sodium sulfate, filtered and concentrated in vacuo to yield 10.35 g of the title compound as oil.
 

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