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[ CAS No. 15058-15-8 ]

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2D
Chemical Structure| 15058-15-8
Chemical Structure| 15058-15-8
Structure of 15058-15-8 *Storage: {[proInfo.prStorage]}

Quality Control of [ 15058-15-8 ]

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Related Doc. of [ 15058-15-8 ]

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Product Details of [ 15058-15-8 ]

CAS No. :15058-15-8MDL No. :MFCD29639081
Formula :C13H8N2OBoiling Point :-
Linear Structure Formula :-InChI Key :GBJXKRIRSDZFGG-UHFFFAOYSA-N
M.W :208.22Pubchem ID :13216164
Synonyms :

Computed Properties of [ 15058-15-8 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 15058-15-8 ]

Signal Word:WarningClassN/A
Precautionary Statements:P261-P305+P351+P338UN#:N/A
Hazard Statements:H302-H315-H319-H335Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 15058-15-8 ]

  • Downstream synthetic route of [ 15058-15-8 ]

[ 15058-15-8 ] Synthesis Path-Downstream   1~10

  • 1
  • [ 15058-15-8 ]
  • [ 744246-71-7 ]
  • 2-(2-{(E)-2-[4-(Methyl-pentadecyl-amino)-phenyl]-vinyl}-chromen-4-ylidene)-malononitrile [ No CAS ]
  • 3
  • [ 15058-15-8 ]
  • 6,6,12,12-tetrakis(4-hexylphenyl)-6,12-dihydrodithieno[2,3-d:2',3'-d’]-s-indaceno[1,2-b:5,6-b’]dithiophene-2,8-dicarboxaldehyde [ No CAS ]
  • C96H86N4O2S4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
With piperidine; In chloroform; acetonitrile; at 80℃; for 24h;Inert atmosphere; The synthesis of IDTT-CMCN proceeded similarly to the synthesis of compound 4, but because of its low solubility in ACN, IDTT-CMCN was synthesized using a mixed solvent of chloroform (CF) and ACN.A mixture of compound 5 (215 mg, 0.2 mmol), compound 2 (41.6 mg, 0.4 mmol) and piperidine (0.1 ml) in a mixed solvent of chloroform and acetonitrile was refluxed at 80 C. for 24 hours under N 2 atmosphere. The mixture was extracted with chloroform, and the extracted organic layer was dried over anhydrous magnesium sulfate (MgSO4) and filtered. After removing the solvent from the filtrate, it was purified by silica gel column chromatography using MC/n-hexane as eluent to obtain a dark purple solid (128 mg, 44%).
  • 7
  • [ 15058-15-8 ]
  • C26H23N3O3 [ No CAS ]
  • 8
  • [ 15058-15-8 ]
  • C31H31N3O5 [ No CAS ]
  • 9
  • [ 15058-15-8 ]
  • [ 122-85-0 ]
  • 2-(2-(4-hydroxystyryl)-4H-chromene-4-ylidene)malononitrile [ No CAS ]
  • 10
  • [ 15058-15-8 ]
  • [ 4181-05-9 ]
  • C32H21N3O [ No CAS ]
YieldReaction ConditionsOperation in experiment
With piperidine; acetic acid; In ethanol; at 80℃; for 12h; (2) Weigh 0.208 g of 2- (2-methyl-4H-chromene-4-methylene) malononitrile (0.1 mol), and 0.273 g of 4- (diphenylamino) benzaldehyde (0.1 mol)Mix the reaction in the presence of piperidine and acetic acid (piperidine: acetic acid = 1: 1) in ethanol solvent, warm to 80 C and reflux for 12 h. After the reaction is completed, the system is filtered by suction to obtain the crude product, which is separated by column chromatography A purified product was obtained, and the mobile phase separated by column chromatography was dichloromethane and petroleum ether with a volume ratio of 1: 5, to obtain a red solid, namely the probe TBM-V:.
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