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Chemical Structure| 1530-89-8 Chemical Structure| 1530-89-8

Structure of 1530-89-8

Chemical Structure| 1530-89-8

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Product Details of [ 1530-89-8 ]

CAS No. :1530-89-8
Formula : C5H8N2O
M.W : 112.13
SMILES Code : N#CN1CCOCC1
MDL No. :MFCD00006164
InChI Key :BOQOXLAQTDFJKU-UHFFFAOYSA-N
Pubchem ID :73738

Safety of [ 1530-89-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302+H312+H332-H315-H319-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 1530-89-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1530-89-8 ]

[ 1530-89-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1530-89-8 ]
  • [ 570-02-5 ]
  • C14H20N2O4 [ No CAS ]
  • 2
  • [ 1530-89-8 ]
  • [ 613-73-0 ]
  • [ 1616963-14-4 ]
YieldReaction ConditionsOperation in experiment
96% With potassium tert-butylate; In 5,5-dimethyl-1,3-cyclohexadiene; at 130℃; for 2h;Inert atmosphere; General procedure: To a solution of 3,3'-((4-methoxybenzyl)azanediyl)dipropanenitrile (130 mg, 0.535 mmol) inxylene (0.3 mL) in a 5 mL reaction tube, the appropriate cyanamide (0.36 mmol) and tBuOK were rapidly added (20 mg, 0.18 mmol). The reaction was heated to 130 C for 2 h andfollowed by TLC using CH2Cl2/MeOH as eluant. After cooling to room temperature, thesolvent was removed and the residue was purified by flash chromatography or HPLC.
 

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