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Chemical Structure| 15330-50-4 Chemical Structure| 15330-50-4

Structure of 15330-50-4

Chemical Structure| 15330-50-4

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Product Details of [ 15330-50-4 ]

CAS No. :15330-50-4
Formula : C9H9N3
M.W : 159.19
SMILES Code : NNC1=CN=CC2=C1C=CC=C2
MDL No. :MFCD19201567

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Application In Synthesis of [ 15330-50-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15330-50-4 ]

[ 15330-50-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 80370-42-9 ]
  • [ 15330-50-4 ]
  • ethyl 1-(isoquinolin-4-yl)-1H-pyrazole-4-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
84% In isopropyl alcohol; at 80℃; A solution consisting of <strong>[80370-42-9]ethyl 2-formyl-3-oxopropanoate</strong> (90.5 mg, 0.628 mmol), 4-hydrazinylisoquinoline, 4a (100 mg, 0.628 mmol) and 2-propanol (2 mL) was stirred at 80 C. overnight before cooling to room temperature and concentrating to dryness under reduced pressure to give the crude product, which was purified by FCC (petroleum ether: ethyl acetate=100:0 to 80:20) to give compound 59a (140 mg, 84%). LCMS (ESI): RT=0.70 min, mass calcd. for C15H13N3O2 267.283, m/z found 268.0 [M+H]+.
 

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