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[ CAS No. 153463-65-1 ]

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Inaccessible (Haz class 6.1), International USD 64.00
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Chemical Structure| 153463-65-1
Chemical Structure| 153463-65-1
Structure of 153463-65-1 * Storage: {[proInfo.prStorage]}

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Product Details of [ 153463-65-1 ]

CAS No. :153463-65-1 MDL No. :MFCD00104651
Formula : C6H2Cl2N2 Boiling Point : 266.2°C at 760 mmHg
Linear Structure Formula :- InChI Key :-
M.W :173.00 g/mol Pubchem ID :11137599
Synonyms :

Safety of [ 153463-65-1 ]

Signal Word:Danger Class:8,6.1
Precautionary Statements:P261-P280-P301+P310-P305+P351+P338 UN#:2923
Hazard Statements:H301-H315-H317-H318-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 153463-65-1 ]

  • Upstream synthesis route of [ 153463-65-1 ]
  • Downstream synthetic route of [ 153463-65-1 ]

[ 153463-65-1 ] Synthesis Path-Upstream   1~7

  • 1
  • [ 917-54-4 ]
  • [ 153463-65-1 ]
  • [ 100868-46-0 ]
  • [ 2457-47-8 ]
  • [ 402561-62-0 ]
Reference: [1] Heterocycles, 2001, vol. 55, # 11, p. 2075 - 2084
  • 2
  • [ 917-64-6 ]
  • [ 153463-65-1 ]
  • [ 100868-46-0 ]
  • [ 402561-62-0 ]
Reference: [1] Heterocycles, 2001, vol. 55, # 11, p. 2075 - 2084
  • 3
  • [ 917-54-4 ]
  • [ 153463-65-1 ]
  • [ 100868-46-0 ]
  • [ 2457-47-8 ]
Reference: [1] Heterocycles, 2001, vol. 55, # 11, p. 2075 - 2084
  • 4
  • [ 153463-65-1 ]
  • [ 22889-78-7 ]
Reference: [1] Heterocycles, 1998, vol. 48, # 6, p. 1203 - 1211
  • 5
  • [ 136590-83-5 ]
  • [ 153463-65-1 ]
YieldReaction ConditionsOperation in experiment
83% With sulfuric acid; hydroxylamine hydrochloride In formic acid for 6 h; Heating / reflux Example 22A; 3,5-dichloro-4-pyridinecarboxaldehyde; A mixture of 3,5-dichloro-4-pyridinecarboxaldehyde (10.0 g, 57.1 mrnol), hydroxylamine hydrochloride (5.25 g 76 mmol), formic acid (50 ml) and H2SO4 cone. (5 drops) was refluxed under N2 for 6 hours The mixture was concentrated under vacuum. The solids were taken in Et2O (250 ml) washed with NaHCO3, brine, organics dried with MgSO4, filtered, concentrated, recrystallized from hexane to give 8.2 g (83percent) of desired nitrile.m.p.ll4°C
Reference: [1] Patent: EP1270577, 2003, A1,
[2] Journal of Medicinal Chemistry, 2005, vol. 48, # 23, p. 7374 - 7388
[3] Patent: WO2006/81072, 2006, A1, . Location in patent: Page/Page column 17; 37
[4] Heterocycles, 1995, vol. 41, # 4, p. 675 - 688
[5] Patent: US6232320, 2001, B1,
[6] Patent: WO2007/14913, 2007, A1, . Location in patent: Page/Page column 101
[7] Patent: WO2007/45588, 2007, A1, . Location in patent: Page/Page column 118-119
[8] Patent: WO2007/93530, 2007, A1, . Location in patent: Page/Page column 248
  • 6
  • [ 70593-51-0 ]
  • [ 153463-65-1 ]
Reference: [1] Bioorganic and Medicinal Chemistry Letters, 2008, vol. 18, # 1, p. 386 - 390
[2] Patent: US2006/178378, 2006, A1, . Location in patent: Page/Page column 16
  • 7
  • [ 183679-35-8 ]
  • [ 153463-65-1 ]
Reference: [1] Heterocycles, 1996, vol. 43, # 9, p. 1893 - 1900
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