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Chemical Structure| 15438-67-2 Chemical Structure| 15438-67-2

Structure of 15438-67-2

Chemical Structure| 15438-67-2

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Product Details of [ 15438-67-2 ]

CAS No. :15438-67-2
Formula : C4H9NO2
M.W : 103.12
SMILES Code : O=C(N)CCOC
MDL No. :MFCD11646082

Safety of [ 15438-67-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 15438-67-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15438-67-2 ]

[ 15438-67-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 15438-67-2 ]
  • [ 100-46-9 ]
  • [ 13304-62-6 ]
YieldReaction ConditionsOperation in experiment
70% With sodium hydroxide; EXAMPLE 23 N-benzylacrylamide 103.1 g (1.0 mole) of 3-methoxypropionamide are heated with 112.5 g (1.05 mole) of benzylamine for 8 hours in a temperature range of 120-170 C. until the evolution of ammonia is complete. The mixture is allowed to cool, 1.5 g of sodium hydroxide are added, and the mixture is heated in a high vacuum at 90-110 C. The methanol is split off within approximately 30 minutes, vigorous foaming occurring. The temperature is increased and 113 g (0.7 mole=70% of the theoretical yield) of N-benzylamide having a Bp0.1 of 112-115 C., which solidifies into crystalline form in the receiver, are distilled off. NMR (CDCl3):delta=4.35 (d,2); 5.35-6.25 (m,3); 7.2 (s,5).
 

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