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Chemical Structure| 15448-58-5 Chemical Structure| 15448-58-5

Structure of 15448-58-5

Chemical Structure| 15448-58-5

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Product Details of [ 15448-58-5 ]

CAS No. :15448-58-5
Formula : C10H6O3
M.W : 174.15
SMILES Code : O=C(C1OC12)C3=C(C=CC=C3)C2=O
MDL No. :MFCD00044300

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Application In Synthesis of [ 15448-58-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 15448-58-5 ]

[ 15448-58-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 15448-58-5 ]
  • [ 111628-39-8 ]
  • 2-[4-(2-Benzoxazolyl)-1-piperazinyl]-3-hydroxy-1,4-naphthalenedione [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; dichloromethane; EXAMPLE 64 2-[4-(2-Benzoxazolyl)-1-piperazinyl]-3-hydroxy-1,4-naphthalenedione A mixture of 3.48 g of 2,3-epoxy-2,3-dihydro-1,4-naphthoquinone, 2.03 g of 2-(1-piperazinyl)benzoxazole and 200 ml of absolute ethanol was stirred for 18 hours and then filtered. The filtrate was concentrated to dryness and the residue flash chromatographed, eluding with dichloromethane, then 1% methanol in dichloromethane. The desired fraction was evaporated, then recrystallized twice from dichloromethane/ethanol, giving 533 mg of the desired product, mp 190 C. (dec.).
 

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