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Chemical Structure| 1547491-85-9 Chemical Structure| 1547491-85-9

Structure of 1547491-85-9

Chemical Structure| 1547491-85-9

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Product Details of [ 1547491-85-9 ]

CAS No. :1547491-85-9
Formula : C30H23N
M.W : 397.51
SMILES Code : C1(C2=CC=C(NC3=CC=C(C4=CC=CC=C4)C=C3)C(C5=CC=CC=C5)=C2)=CC=CC=C1
MDL No. :MFCD32670217
InChI Key :KIHBHETWBSJUJO-UHFFFAOYSA-N
Pubchem ID :86762383

Safety of [ 1547491-85-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 1547491-85-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1547491-85-9 ]

[ 1547491-85-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 50548-45-3 ]
  • [ 1547491-85-9 ]
  • C42H29NO [ No CAS ]
YieldReaction ConditionsOperation in experiment
71% With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate; In 5,5-dimethyl-1,3-cyclohexadiene; for 7h;Inert atmosphere; Reflux; To a 500 ml round bottom flask in a nitrogen atmosphereCompound 1-Bromobenzofuran (10.0 g, 40.65 mmol),1,1'-biphenyl] -4-yl) - [1,1 ': 3', 1 '' - terphenyl(N - ([1,1'-biphenyl] -4-yl) - [1,1 ': 3', 1 '' - terphenyl]"(17.75 g, 44.72 mmol) Xylene(Xylene) in 260 mlAfter completely dissolvedSodium tert-butoxide(sodium tertbutoxide) (5.08 g, 52.85 mol) was added,Bis (tri-tert-butylphosphine) palladium (0)(Bis (tri-tert-butylphosphine) palladium (0)) (0.21 g, 0.41 mmol)And the mixture was heated and stirred for 7 hours.The temperature was lowered to room temperature and filteredAfter the salt was removed, xylene was concentrated under reduced pressure and recrystallized from ethyl acetate (200 ml) to obtain Compound (3) (16.17 g, yield: 71percent).
 

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