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Chemical Structure| 157427-49-1 Chemical Structure| 157427-49-1

Structure of 157427-49-1

Chemical Structure| 157427-49-1

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Product Details of [ 157427-49-1 ]

CAS No. :157427-49-1
Formula : C16H15N
M.W : 221.30
SMILES Code : CC1=CC=CC=C1C(N2C)=CC3=C2C=CC=C3
MDL No. :MFCD31231815

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Application In Synthesis of [ 157427-49-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 157427-49-1 ]

[ 157427-49-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 603-76-9 ]
  • [ 615-37-2 ]
  • [ 157427-49-1 ]
YieldReaction ConditionsOperation in experiment
80% With 2,6-bis[(N-phenyl)imino]phenylpalladium bromide; potassium acetate; at 80℃; for 24h; General procedure: A mixture of indole (0.13 g, 1 mmol), aryl halide (1.5 mmol),KOAc (2 mmol), catalyst (1 mg, 1 mol%) and DMAc (3 mL) werestirred at 110 C for 24 h. After cooling to room temperature, the mixture was diluted with ethyl acetate (5 mL) and filtered. The liquid phase was washed with deionized water and dried over Na2SO4. The solvent was removed under reduced pressure and the residue was further purified by chromatography on silica gel (n-hexane/ethyl acetate) to give the desired product. All products were known compounds and were identified by comparison of their physical and spectra data with those of authentic samples.
 

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