Home Cart Sign in  
Chemical Structure| 16218-30-7 Chemical Structure| 16218-30-7

Structure of 16218-30-7

Chemical Structure| 16218-30-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 16218-30-7 ]

CAS No. :16218-30-7
Formula : C13H6I2O
M.W : 432.00
SMILES Code : O=C1C2=C(C3=C1C=C(I)C=C3)C=CC(I)=C2
MDL No. :MFCD00184950
Boiling Point : No data available

Safety of [ 16218-30-7 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H318-H411
Precautionary Statements:P280-P305+P351+P338+P310
Class:9
UN#:3077
Packing Group:

Application In Synthesis of [ 16218-30-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 16218-30-7 ]

[ 16218-30-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 902518-11-0 ]
  • [ 16218-30-7 ]
  • 2,7-diiodospiro[fluorene-9,8'-indolo[3,2,1-de]acridine] [ No CAS ]
YieldReaction ConditionsOperation in experiment
25% In a 250 mL two-necked flask, 9- (2-bromophenyl) -9H-carbazole (1.98 g, 6.15 mmol) was dissolved in 50 mL of THF. After cooling to -78°C, n-BuLi (2.5 M in hexane, 2.58 mL, 6.45 mmol) was slowly added dropwise. After 2 hours, 2,7-diiodo-9H-fluoren-9-one (2.65 g, 6.15 mmol) was added. After 3 hours, the reaction was terminated with aqueous NH4Cl solution and diethyl Ether. The water was dried over MgSO4 and the solvent was removed. After precipitation with ethanol, the solid was filtered. The resulting solid was dissolved in acetic acid (50 mL), and a catalytic amount of HCl was added. The mixture was refluxed for 6 hours and then cooled to room temperature. The resulting solid was filtered, washed with ethanol and dried to obtain 1.0 g (25percent) of a white solid.
 

Historical Records

Technical Information

Categories