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[ CAS No. 1634-34-0 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 1634-34-0
Chemical Structure| 1634-34-0
Chemical Structure| 1634-34-0
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Product Details of [ 1634-34-0 ]

CAS No. :1634-34-0 MDL No. :MFCD06656138
Formula : C9H10O3 Boiling Point : -
Linear Structure Formula :- InChI Key :CUYUORWXJSURNV-UHFFFAOYSA-N
M.W : 166.17 Pubchem ID :10419531
Synonyms :

Safety of [ 1634-34-0 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1634-34-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 1634-34-0 ]
  • Downstream synthetic route of [ 1634-34-0 ]

[ 1634-34-0 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 1634-34-0 ]
  • [ 17773-10-3 ]
  • [ 2260-50-6 ]
YieldReaction ConditionsOperation in experiment
93% at 65℃; for 2 h; Add 3 mol of 3,5-dihydroxy-4-acetyltoluene and 5 mol of iodocholine to the reaction vessel to control the stirring speed.130rpm, raise the temperature to 65 ° C, maintain the temperature and continue to stir until completely dissolved, let stand for 120min, reduce the solution temperatureThe crystal was precipitated to 15 ° C, filtered, and the crystal was washed with a cyclohexane solution having a mass fraction of 85percent, and the mass fraction was 90percent.The toluene solution was washed, and the anhydrous potassium carbonate dehydrating agent was dehydrated to obtain 761.67 g of the finished iodoacetylcholine, and the yield was 93percent
Reference: [1] Patent: CN108250089, 2018, A, . Location in patent: Paragraph 0011; 0013; 0015
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