Structure of Tribenzylsilane
CAS No.: 1747-92-8
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| CAS No. : | 1747-92-8 |
| Formula : | C21H22Si |
| M.W : | 302.48 |
| SMILES Code : | [SiH](CC1=CC=CC=C1)(CC2=CC=CC=C2)CC3=CC=CC=C3 |
| MDL No. : | MFCD00004769 |
| InChI Key : | QXZGXRIXJAVMTI-UHFFFAOYSA-N |
| Pubchem ID : | 6330251 |
| GHS Pictogram: |
|
| Signal Word: | Warning |
| Hazard Statements: | H315-H319 |
| Precautionary Statements: | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

| Yield | Reaction Conditions | Operation in experiment |
|---|---|---|
| 73% | (f) Preparation of tribenzylsilane By reacting sodium tris(benzene-1,2-diolato)silicate with 3 equivalents of benzylmagnesium bromide under the above conditions, tribenzylsilane of the formula: STR15 is obtained with a yield of 73%. |
| Yield | Reaction Conditions | Operation in experiment |
|---|---|---|
| 80% | With silver(I) acetate; In acetonitrile; at 120℃; for 26.0h; | AgOAc (0.25 mmol, 0.0414 g) was added to the reaction flask, acetonitrile (MeCN, 2.5 ml) was added, and then 2.5 mmol of compound 1e (0.7554 g) was slowly added to the reaction flask, and the reaction was stirred at 120 C for 24 After 2 hours, the product 2e (0.6025 g) was distilled off under reduced pressure after the reaction was completed, and the yield was 80%. |
[ 1747-92-8 ]
[ 201338-62-7 ]