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Chemical Structure| 50-30-6 Chemical Structure| 50-30-6
Chemical Structure| 50-30-6

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Product Details of 2,6-Dichlorobenzoic Acid

CAS No. :50-30-6
Formula : C7H4Cl2O2
M.W : 191.01
SMILES Code : O=C(O)C1=C(Cl)C=CC=C1Cl
MDL No. :MFCD00002418
InChI Key :MRUDNSFOFOQZDA-UHFFFAOYSA-N
Pubchem ID :5758

Safety of 2,6-Dichlorobenzoic Acid

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of 2,6-Dichlorobenzoic Acid

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 50-30-6 ]

[ 50-30-6 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 25185-95-9 ]
  • [ 50-30-6 ]
  • 2
  • [ 129999-60-6 ]
  • [ 50-30-6 ]
  • [ 948895-18-9 ]
YieldReaction ConditionsOperation in experiment
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20℃; for 14h; Example 44; s 2,6-Dichloro-iV-[2-(4-[(2i?)-2-hydroxy-2-(8-hydroxy-2-oxo-l,2-dihydroquinolin-5- yl)ethyl]amino}piperidin-l-yl)ethyl]benzamide; i) 2,6-Dichloro-iV-[2-(4-hydroxypiperidin-l-yl)ethyl]benzamideA solution of l-(2-aminoethyl)piperidm-4-ol (0.312 g), 2,6-dichlorobenzoic acid (0.826g), 0 and triethylamine (0.61 mL) in DMF (10 mL) was treated with PyBROP (1.2Ig) at ambient temperature. After stirring for 14 h the mixture was loaded onto a SCX cartridge and eluted with acetonitrile followed by methanol. The product was then eluted off with ammonia/methanol solutions to give the subtitle compound, after solvent evaporation, as a yellow oil. Yield: 0.7g s MS APCI+ 317/319/321 [M+H]+
  • 3
  • [ 50-30-6 ]
  • [ 25185-95-9 ]
 

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