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[ CAS No. 25185-95-9 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 25185-95-9
Chemical Structure| 25185-95-9
Chemical Structure| 25185-95-9
Structure of 25185-95-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 25185-95-9 ]

CAS No. :25185-95-9 MDL No. :MFCD00013938
Formula : C7H5Cl2NO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 190.03 Pubchem ID :-
Synonyms :

Safety of [ 25185-95-9 ]

Signal Word:Danger Class:4.1,6.1
Precautionary Statements:P280-P210-P240-P264-P270-P301+P310-P330-P370+P378-P403+P233-P405-P501 UN#:2926
Hazard Statements:H228-H301-H315-H319-H335-H372 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 25185-95-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 25185-95-9 ]
  • Downstream synthetic route of [ 25185-95-9 ]

[ 25185-95-9 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 25185-95-9 ]
  • [ 6575-27-5 ]
YieldReaction ConditionsOperation in experiment
94% With iron oxide; zirconium(IV) chloride; sodium cyanoborohydride In neat (no solvent) at 75 - 80℃; for 1 h; General procedure: A mixture of benzaldehyde oxime (0.121 g, 1 mmol) and nano Fe3O4 (0.046 g, 0.2 mmol) (nano particle size≈70 nm) was ground in a porcelain mortar. ZrCl4 (0.233 g,1 mmol) was then added and grinding the mixture was continued for a moment at room temperature. The mortar was heated in an oil bath until the temperature of reaction mixture reaches 75–80 °C. NaBH3CN (0.314 g, 5 mmol) wasthen added portion wisely and the mixture was ground for15 min at 75–80 °C. After completion of the reaction, H2O(5 mL) was added and the mixture was stirred for 5 min. The mixture was extracted with EtOAc (2 × 5 mL) and then dried over anhydrous Na2SO4. Evaporation of the solvent affords the pure liquid benzylamine in 93 percent yield (0.1 g, Table 2, entry 1).
Reference: [1] Journal of the Iranian Chemical Society, 2015, vol. 12, # 5, p. 873 - 878
[2] Journal of Medicinal Chemistry, 1984, vol. 27, # 9, p. 1111 - 1118
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