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Chemical Structure| 202197-73-7 Chemical Structure| 202197-73-7

Structure of 202197-73-7

Chemical Structure| 202197-73-7

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Product Details of [ 202197-73-7 ]

CAS No. :202197-73-7
Formula : C9H6N2O3
M.W : 190.16
SMILES Code : O=C(C1=CC(N=CN2)=C(C=C1)C2=O)O
MDL No. :MFCD03942331
InChI Key :ICASWNVSUDFGRH-UHFFFAOYSA-N
Pubchem ID :135483588

Safety of [ 202197-73-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 202197-73-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 202197-73-7 ]

[ 202197-73-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • [ 202197-73-7 ]
  • [ 313535-84-1 ]
YieldReaction ConditionsOperation in experiment
86% With sulfuric acid; at 60℃; for 11h; To a solution of 4-oxo-3,4-dihydroquinazoline-7-carboxylic acid (3.30g, 14.8 mmol) in 60 mL methanol was added 6.6 mL of sulfuric acid. The resulting mixture was stirred at 60 C for 11 hours. After cooled to room temperature, the solvent was removed in vacuo and the residue was diluted with water. Aqueous sodium hydroxide (6 mol/L) was added to adjust the pH value to 8 and the precipitated solid was collected by filtration. The filter cake was washed with water and dried in oven to give 3.00 g (86%) of the product as a light yellow solid. MS (ESIpos): m/z = 205 (M+H)+. LC-MS [Method 2]: Rt = 0.67 min.
 

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Related Functional Groups of
[ 202197-73-7 ]

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