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Chemical Structure| 20265-96-7 Chemical Structure| 20265-96-7

Structure of 20265-96-7

Chemical Structure| 20265-96-7

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Product Details of [ 20265-96-7 ]

CAS No. :20265-96-7
Formula : C6H7Cl2N
M.W : 164.03
SMILES Code : NC1=CC=C(Cl)C=C1.[H]Cl
MDL No. :MFCD00042057
InChI Key :ISJBQSJDQZLCSF-UHFFFAOYSA-N
Pubchem ID :5284363

Safety of [ 20265-96-7 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H300+H310+H330-H350-H360
Precautionary Statements:P260-P262-P264-P270-P271-P280-P284-P301+P310+P330-P302+P352+P310+P361+P364-P304+P340+P310-P403+P233-P405-P501
Class:6.1
UN#:2811
Packing Group:

Application In Synthesis of [ 20265-96-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 20265-96-7 ]

[ 20265-96-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1005-39-6 ]
  • [ 20265-96-7 ]
  • [ 103853-50-5 ]
  • 2
  • [ 20265-96-7 ]
  • [ 101094-85-3 ]
  • [ 212141-54-3 ]
YieldReaction ConditionsOperation in experiment
In ethanol; for 2h;Heating / reflux;Product distribution / selectivity; A mixture of 0.972 g (3.8 mmol) l-chloro-4-(4- pyridylmethyl)phthalazine, 0.656 g (4 mmol) 4-chloroaniline hydrochloride (Research Organics, Inc., Cleveland, Ohio, USA) and 20 ml ethanol is heated for 2 h under reflux. The reaction mixture is cooled in an ice bath, filtered, and the crystallizate washed with a little ethanol and ether. After drying under HV for 8 h at 110 C. and for 10 h at 150 C, the title compound is obtained as a result of thermal removal of HCl; m.p. >270 C; ' H NMR (DMSO-d 6 ) 9.80-11.40 (br), 8.89-8.94 (m, IH), 8.67 (d, 2H), 8.25-8.30 (m, IH), 8.06-8.17 (m, 2H), 7.87 (d, 2H), 7. 69 (d, 2H), 7.49 (d, 2H), 4.81 (s, 2H); ESI-MS: (M+H) +=347.
 

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