Alternatived Products of [ 20306-75-6 ]
Product Details of [ 20306-75-6 ]
CAS No. : | 20306-75-6 |
MDL No. : | MFCD00044026 |
Formula : |
C5H9NO2
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
115.13
|
Pubchem ID : | - |
Synonyms : |
|
Application In Synthesis of [ 20306-75-6 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 20306-75-6 ]
- 1
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[ 20306-75-6 ]
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[ 74877-07-9 ]
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[ 132361-84-3 ]
- 2
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[ 20306-75-6 ]
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[ 74788-46-8 ]
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[ 132361-85-4 ]
- 3
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[ 107292-92-2 ]
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[ 10128-60-6 ]
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[ 105-40-8 ]
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[ 20306-75-6 ]
- 4
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[ 20306-75-6 ]
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[ 43192-33-2 ]
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4-(4-Bromo-2-methoxy-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid bis-methylamide
[ No CAS ]
- 5
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[ 4116-10-3 ]
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[ 20306-75-6 ]
Yield | Reaction Conditions | Operation in experiment |
100% |
With potassium carbonate; para-thiocresol In acetonitrile at 20℃; for 0.75h; Sonication; |
General procedure: A mixture of α-halocarbony1 compound (1.0 mmol), thiol(2.25 mmol), potassium salt (1.2 mmol) in acetonitrile (5 mL)was stirred at room temperature and in the open atmospherein a glass reactor. The completion of reaction was monitoredby TLC. The reaction mixture was filtered, and evaporation ofthe filtrate under reduced pressure followed by preparative thinlayer chromatography on silica gel afforded the pure products.Among them, compounds 2b and 2c are new. |
Reference:
[1]Dong, Wei-Li; Cai, Wen-Xi; Wu, Rui; Li, Zheng-Ming; Zhao, Wei-Guang; Liu, Xing-Hai
[Phosphorus, Sulfur and Silicon and the Related Elements, 2016, vol. 191, # 7, p. 980 - 983]
- 6
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[ 20306-75-6 ]
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[ 4116-10-3 ]
Yield | Reaction Conditions | Operation in experiment |
|
With sulfuryl dichloride In toluene at 20℃; for 4h; |
General procedure: The α-halocarbony1 compound was prepared accordingto the literature.24 To a solution of 3-oxo-N,3-disubstitutedpropanamide(0.0722 mol) in toluene (80 mL),was added sulfuryl dichloride (0.0722 mol) at 20 °C, then themixture was stirred for 4 h. After the reaction is completed,the solvent was moved and the solid was recrystallized inPE/EA(v/v = 1:1). |
Reference:
[1]Dong, Wei-Li; Cai, Wen-Xi; Wu, Rui; Li, Zheng-Ming; Zhao, Wei-Guang; Liu, Xing-Hai
[Phosphorus, Sulfur and Silicon and the Related Elements, 2016, vol. 191, # 7, p. 980 - 983]
- 7
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[ 20306-75-6 ]
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[ 366496-33-5 ]
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C11H9BrN2O4
[ No CAS ]
- 8
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[ 20306-75-6 ]
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[ 366496-33-5 ]
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C11H10Br2N2O4
[ No CAS ]