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Chemical Structure| 20927-96-2 Chemical Structure| 20927-96-2

Structure of 20927-96-2

Chemical Structure| 20927-96-2

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Product Details of [ 20927-96-2 ]

CAS No. :20927-96-2
Formula : C13H7NO
M.W : 193.20
SMILES Code : N#CC1=CC=C2OC3=CC=CC=C3C2=C1
MDL No. :MFCD00092383
InChI Key :JMLMVVOQPAPVOQ-UHFFFAOYSA-N
Pubchem ID :4102983

Safety of [ 20927-96-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319
Precautionary Statements:P264-P280-P302+P352-P305+P351+P338-P332+P313-P337+P313-P362

Application In Synthesis of [ 20927-96-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 20927-96-2 ]

[ 20927-96-2 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 3096-81-9 ]
  • [ 20927-96-2 ]
  • 2
  • [ 2296-23-3 ]
  • [ 98-80-6 ]
  • [ 20927-96-2 ]
  • 3
  • [ 5408-56-0 ]
  • potassium ferrocyanide [ No CAS ]
  • [ 20927-96-2 ]
YieldReaction ConditionsOperation in experiment
77% With Cu2O/SBA-15; In N,N-dimethyl-formamide; at 120℃; for 8h; Synthesis of intermediate 2-61-3:450 ml of DMF and 43.51 g of <strong>[5408-56-0]2-iododibenzofuran</strong> were added to the three-necked flask.193g K4[Fe(CN)6], 400mg Cu2O/SBA-15,The reaction was carried out at 120 C for 8 h, and the basic reaction of the raw materials was determined by HPLC.After cooling to room temperature, the reaction solution was dried under reduced pressure.The residue was subjected to column chromatography to give 26.2 g of Intermediate 2-61-3(yield 77%)
 

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