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[ CAS No. 213453-08-8 ] {[proInfo.proName]}

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3d Animation Molecule Structure of 213453-08-8
Chemical Structure| 213453-08-8
Chemical Structure| 213453-08-8
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Product Details of [ 213453-08-8 ]

CAS No. :213453-08-8 MDL No. :MFCD18785732
Formula : C10H15BrO4 Boiling Point : -
Linear Structure Formula :- InChI Key :QXDYJUSFCUKOQD-UHFFFAOYSA-N
M.W : 279.13 Pubchem ID :21216988
Synonyms :

Safety of [ 213453-08-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P264-P270-P301+P312-P330-P501 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 213453-08-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 213453-08-8 ]

[ 213453-08-8 ] Synthesis Path-Downstream   1~20

  • 1
  • [ 868-77-9 ]
  • [ 20769-85-1 ]
  • [ 213453-08-8 ]
YieldReaction ConditionsOperation in experiment
The 2-(bromoisobutyryloxy)ethyl methacrylate (BIEM, 2b) monomer was synthesized using a modified method following a previous report.4 In a typical run, HEMA (5.0 g, 0.038 mol) and triethylamine (7.8 g, 0.077 mol) were dissolved in dichloromethane (48.9 g, 0.6 mol) in a round-bottomed Schlenk flask under nitrogen. The reaction mixture was stirred at 0 C. and degassed by N2 for 45 min. α-bromoisobutyryl bromide (10.6 g, 0.046 mol) was then added drop-wise over a period of 20 min. After the reaction mixture was stirred for another 6 h at 0 C., the insoluble solids were filtered off. The filtrate was washed three times each with de-ionized water (3×50 mL), 0.5 M NaHCO3 (3×50 mL) and saturated NaCl (3×50 mL) aqueous solutions, respectively. Subsequently, MgSO4 was added to remove trace water and filtered off. The filtrate was evaporated to dryness. The final product, BIEM (2b), was further dried in a vacuum oven and its structure was confirmed by 1H NMR (FIG. 13A).
  • 2
  • [ 105-16-8 ]
  • [ 213453-08-8 ]
  • polymer, Mn 5700 and Mw/Mn 1.88 by GPC, Mn 7900 and Mw/Mn 3.90 by GPC/viscosimetry; monomer(s): 2-(diethylamino)ethyl methacrylate; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 3
  • [ 105-16-8 ]
  • [ 213453-08-8 ]
  • polymer; monomer(s): 2-(2-bromoisobutyryloxy)ethyl methacrylate; 2-(diethylamino)ethyl methacrylate [ No CAS ]
  • 4
  • [ 105-16-8 ]
  • [ 213453-08-8 ]
  • polymer, Mn 13100 and Mw/Mn 1.36 by GPC/viscosimetry, Mn 6800 and Mw/Mn 2.00 by GPC; monomer(s): 2-(2-bromoisobutyryloxy)ethyl methacrylate; 2-(diethylamino)ethyl methacrylate [ No CAS ]
  • 5
  • [ 105-16-8 ]
  • [ 213453-08-8 ]
  • polymer, Mn 3600 and Mw/Mn 1.76 by GPC, Mn 6300 and Mw/Mn 2.75 by GPC/viscosimetry; monomer(s): 2-(diethylamino)ethyl methacrylate; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 6
  • [ 105-16-8 ]
  • [ 213453-08-8 ]
  • polymer, Mn 4500 and Mw/Mn 1.58 by GPC, Mn 6200 and Mw/Mn 2.80 by GPC/viscosimetry; monomer(s): 2-(diethylamino)ethyl methacrylate; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 7
  • [ 105-16-8 ]
  • [ 213453-08-8 ]
  • polymer, Mn 30100 and Mw/Mn 1.70 by GPC, Mn 35600 and Mw/Mn 1.21 by GPC/viscosimetry; monomer(s): 2-(diethylamino)ethyl methacrylate; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 8
  • [ 213453-08-8 ]
  • poly(2-(2-bromoisobutyryloxy)ethyl methacrylate), Mn 30900 and Mw/Mn 1.66 by GPC/viscosimetry, Mn 9000 and Mw/Mn 1.32 by GPC, Mn 25000 by 1H NMR; monomer(s): 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 9
  • [ 213453-08-8 ]
  • poly(2-(2-bromoisobutyryloxy)ethyl methacrylate), Mn 14800 and Mw/Mn 5.51 by GPC; monomer(s): 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 10
  • [ 213453-08-8 ]
  • poly(2-(2-bromoisobutyryloxy)ethyl methacrylate), Mn 14800 and PDI 5.51 by GPC; monomer(s): 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 11
  • 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose [ No CAS ]
  • [ 213453-08-8 ]
  • polymer, branched, Mn 9800 Da by GPC, Mn 13700 Da by GPC/viscosity, PDI 1.64 by GPC, PDI 1.50 by GPC/viscosity; monomer(s): 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 12
  • 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose [ No CAS ]
  • [ 213453-08-8 ]
  • polymer, branched, Mn 6300-9300 Da by GPC, Mn 17500 Da by GPC/viscosity, PDI 1.45-1.81 by GPC, PDI 2.01 by GPC/viscosity; monomer(s): 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 13
  • 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose [ No CAS ]
  • [ 213453-08-8 ]
  • polymer, branched, Mn 7900 Da by GPC, Mn 17600 Da by GPC/viscosity, PDI 1.94 by GPC, PDI 2.12 by GPC/viscosity; monomer(s): 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 14
  • 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose [ No CAS ]
  • [ 213453-08-8 ]
  • polymer, branched, Mn 9500 Da by GPC, Mn 18000 Da by GPC/viscosity, PDI 1.75 by GPC, PDI 1.85 by GPC/viscosity; monomer(s): 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 15
  • 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose [ No CAS ]
  • [ 213453-08-8 ]
  • polymer, branched, Mn 6700-10100 Da by GPC, Mn 21000 Da by GPC/viscosity, PDI 1.51-1.53 by GPC, PDI 1.55 by GPC/viscosity; monomer(s): 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 16
  • 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose [ No CAS ]
  • [ 213453-08-8 ]
  • polymer, branched, Mn 7700-11100 Da by GPC, Mn 23300 Da by GPC/viscosity, PDI 1.43-1.53 by GPC, PDI 1.57 by GPC/viscosity; monomer(s): 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 17
  • 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose [ No CAS ]
  • [ 213453-08-8 ]
  • polymer, branched, Mn 15400 Da by GPC, Mn 29800 Da by GPC/viscosity, PDI 1.44 by GPC, PDI 1.71 by GPC/viscosity; monomer(s): 3-O-methacryloyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose; 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 18
  • [ 213453-08-8 ]
  • poly(2-(2-bromoisobutyryloxy)ethyl methacrylate); monomer(s): 2-(2-bromoisobutyryloxy)ethyl methacrylate [ No CAS ]
  • 20
  • [ 868-77-9 ]
  • [ 33693-78-6 ]
  • [ 213453-08-8 ]
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