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CAS No. : | 223376-47-4 | MDL No. : | MFCD11506115 |
Formula : | C8H7N3O | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | CZXPBOPRQAPKGX-UHFFFAOYSA-N |
M.W : | 161.16 | Pubchem ID : | 44608104 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With ammonium hydroxide; In methanol; at 80℃; | To a solution of methyl 1 H-pyrrolo[2,3-b]pyridine-2-carboxylate (H-1 ) (880 mg, 5.0 mmol) in MeOH (2 mL) was added NH3.H20 (6 ml_). The reaction was heated at 80C overnight. After being cooled to room temparature, the mixture was concentrated in vacuo to afford the title compound (805 mg) as a yellow solid, which was used for the next step without further purification. MS (m/z): 162 (M-M )+. | |
With ammonium hydroxide; In methanol; at 80℃; | 1H-Pyrrolo[2,3-b]pyridine-2-carboxamide (H-2) To a solution of <strong>[394223-02-0]methyl 1H-pyrrolo[2,3-b]pyridine-2-carboxylate</strong> (H-1) (880 mg, 5.0 mmol) in MeOH (2 mL) was added NH3.H2O (6 mL). The reaction was heated at 80 C. overnight. After being cooled to room temperature, the mixture was concentrated in vacuo to afford the title compound (805 mg) as a yellow solid, which was used for the next step without further purification. MS (m/z): 162 (M+1)+. |
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