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Chemical Structure| 23046-68-6 Chemical Structure| 23046-68-6

Structure of 23046-68-6

Chemical Structure| 23046-68-6

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Product Details of [ 23046-68-6 ]

CAS No. :23046-68-6
Formula : C11H12Cl2N2
M.W : 243.13
SMILES Code : ClC1=CC(C2=C(CNCC2)N3)=C3C=C1.[H]Cl
MDL No. :MFCD09997625
InChI Key :SXHJWBRJNQZWBI-UHFFFAOYSA-N
Pubchem ID :3159695

Safety of [ 23046-68-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 23046-68-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 23046-68-6 ]

[ 23046-68-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3621-82-7 ]
  • [ 23046-68-6 ]
  • 6-chloro-2-(6-chloro-1,3-benzoxazol-2-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole [ No CAS ]
YieldReaction ConditionsOperation in experiment
39% With potassium carbonate; In N,N-dimethyl-formamide; for 12h; General procedure: Method A:41 To a round bottom flask was added tryptoline (21mg, 0.100mmol), 2-chlorobenzothiazole (31mg, 0.150mmol), K2CO3 (70mg, 0.500mmol) and DMF (2.0mL), and the reaction mixture was stirred for 12h at 110C. After the reaction was then cooled to room temperature, ethyl acetate (10mL) and H2O (10mL) were added into the mixture, and the aqueous layer was extracted with 2×10mL ethyl acetate. The organic layer then was combined and washed with brine, and dried over Na2SO4. The solvents were removed under vacuum, and the residue was purified by flash chromatography on silica gel using ethyl acetate/hexane as eluent.
 

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