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Chemical Structure| 23585-55-9 Chemical Structure| 23585-55-9

Structure of 23585-55-9

Chemical Structure| 23585-55-9

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Product Details of [ 23585-55-9 ]

CAS No. :23585-55-9
Formula : C5H8N2O
M.W : 112.13
SMILES Code : CC(O)C1=CNN=C1
MDL No. :MFCD16862655

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Application In Synthesis of [ 23585-55-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 23585-55-9 ]

[ 23585-55-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 23585-55-9 ]
  • [ 28466-26-4 ]
YieldReaction ConditionsOperation in experiment
42% With sodium azide; methanesulfonic acid; trifluoroacetic acid; In hexane; at 40℃; for 12h; Take a reaction tube, add 50 mg of sodium azide, 33.6 mg of 1-(4-pyrazolyl)ethanol, and 300 uL of trifluoroacetic acid.150 uL of methanesulfonic acid and 1.0 mL of n-hexane were stirred at 40 C for 12 hours.After the reaction was completed, 10 mL of a sodium hydroxide solution was added to quench the reaction, and the mixture was extracted three times with ethyl acetate.Column chromatography yielded 10.5 mg of 4-aminopyrazole in a yield of 42%.
 

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