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Chemical Structure| 2386-60-9 Chemical Structure| 2386-60-9

Structure of 2386-60-9

Chemical Structure| 2386-60-9

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Product Details of [ 2386-60-9 ]

CAS No. :2386-60-9
Formula : C4H9ClO2S
M.W : 156.63
SMILES Code : CCCCS(=O)(Cl)=O
MDL No. :MFCD00007464
InChI Key :WEDIIKBPDQQQJU-UHFFFAOYSA-N
Pubchem ID :75430

Safety of [ 2386-60-9 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314-H335
Precautionary Statements:P261-P280-P305+P351+P338-P310
Class:8
UN#:3265
Packing Group:

Application In Synthesis of [ 2386-60-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2386-60-9 ]

[ 2386-60-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 2386-60-9 ]
  • [ 120-35-4 ]
  • 3-(Butane-1-sulfonylamino)-4-methoxy-N-phenyl-benzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
Example 129 3-(Butane-1-sulfonylamino)-4-methoxy-N-phenyl-benzamide Prepared according to the procedure described for Example 128 using 1-butanesulfonyl chloride (0.47 g, 3.0 mmol) and 3-amino-4-methoxy-N-phenyl-benzamide (0.73 g, 3.0 mmol) to afford the product (1.0 g); m.p. 182-183 C. after recrystallization from ethanol. Calculated for C18H22N2O4S: C, 59.65; H, 6.12; N, 7.73. Found: C, 59.68; H, 6.09; N, 7.60.
  • 2
  • [ 6174-86-3 ]
  • [ 2386-60-9 ]
  • 3-chloro-4-methyl-2-oxo-2H-chromen-7-yl butane-1-sulfonate [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% With triethylamine; In tetrahydrofuran; at 20℃; for 4h; General procedure: Coumarin sulfonates 1-38 were synthesized by reactingdifferent hydroxylated coumarin derivatives (1 mmol) withcommercially available sulfonyl chlorides derivatives (1.2 mmol) inTHF (15 mL) and triethyl amine (1 mmol) was used as base. Reactionmixture was stirred for 4 h at room temperature to afford avariety of coumarin sulfonate esters 1e38. TLC monitoring wasused to determine the progress of the reaction. After the completionof reaction, THF was evaporated under reduced pressure andthe solid product obtained was washed with distilled water anddried under vacuum. The products were recrystallized in methanoland gave good yields. All the synthetic compounds 1-38 werecharacterized by different spectroscopic techniques such as EI-MS,HREI-MS, 1H-NMR, and 13C-NMR.
 

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