Alternatived Products of [ 2393-20-6 ]
Alternatived Products of [ 2393-20-6 ]
Product Details of [ 2393-20-6 ]
CAS No. : | 2393-20-6 | MDL No. : | MFCD03410969 |
Formula : |
C8H9NO2
|
Boiling Point : |
278.7°C at 760 mmHg |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 151.16 | Pubchem ID : | - |
Synonyms : |
|
Computed Properties of [ 2393-20-6 ]
TPSA :Topological Polar Surface Area |
- |
H-Bond Acceptor Count : |
- |
XLogP3 : |
- |
H-Bond Donor Count : |
- |
SP3 : |
- |
Rotatable Bond Count : |
- |
Application In Synthesis of [ 2393-20-6 ]
- Upstream synthesis route of [ 2393-20-6 ]
- Downstream synthetic route of [ 2393-20-6 ]
- 1
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[ 64-17-5 ]

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[ 2393-20-6 ]

-
[ 366-84-7 ]
Yield | Reaction Conditions | Operation in experiment |
|
With thionyl chloride; In acetic acid; at 0 - 20℃; for 8h; |
Measure 10 ml of ethanol in the reaction flask,Add 0.4g of 3-aminomethylbenzoic acid,After stirring and dissolving,Slowly add thionyl chloride at 0 C.After the drop,Raise the reaction to room temperature for 8 h,After the reaction is completed, the solvent is distilled off under reduced pressure, and saturated sodium hydrogen carbonate solution is adjusted.The pH is adjusted to 7-8, ethyl acetate is extracted, washed with saturated brine, dried over anhydrous sodium sulfate |