Home Cart Sign in  
Chemical Structure| 2430-16-2 Chemical Structure| 2430-16-2

Structure of 2430-16-2

Chemical Structure| 2430-16-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 2430-16-2 ]

CAS No. :2430-16-2
Formula : C12H18O
M.W : 178.27
SMILES Code : OCCCCCCC1=CC=CC=C1
MDL No. :MFCD00014063

Safety of [ 2430-16-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 2430-16-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2430-16-2 ]

[ 2430-16-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2430-16-2 ]
  • [ 4983-28-2 ]
  • 2-chloro-5-((6-phenylhexyl)oxy)pyrimidine [ No CAS ]
YieldReaction ConditionsOperation in experiment
72% With di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; at 0 - 20℃; for 24h; Step 1. 2-chloro-5-((6-phenylhexyl)oxy)pyrimidine. To a stirring solution of chlorohydroxypyrimidine (250 mg, 1.92 mmol), 6-phenylhexanol (444 mg, 2.5 mmol), in THF (5 mL) was added DIEA (1.0 mL, 5.76 mmol), PPh3 (1.0 g, 3.84 mmol) and the mixture was cooled to 0 °C and DIAD (0.756 mL, 3.84 mmol) was added dropwise. The mixture was allowed to warm to rt and stirred for 24h. The crude reaction mixture was concentrated, and purified by silica gel chromatography using 0-10percent EtOAc/hexanes to afford 2-chloro-5-((6-phenylhexyl)oxy)pyrimidine as a white solid (400 mg, 72percent): XH NMR (500MHz, CDCl3) delta ppm 8.26 (s, 2H), 7.15 - 7.30 (m, 5H), 4.03 (t, J= 6.3 Hz, 2H), 2.63 (t, J= 7.8 Hz, 2H), 1.81 (quin, J= 8.3 Hz, 2H), 1.66 (quin, J= 7.7 Hz, 2H), 1.49 (quin, J= 7.8 Hz, 2H), 1.40 (J= 7.8 Hz, 2H).
 

Historical Records

Technical Information

Categories