Home Cart Sign in  
Chemical Structure| 24446-27-3 Chemical Structure| 24446-27-3

Structure of 24446-27-3

Chemical Structure| 24446-27-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 24446-27-3 ]

CAS No. :24446-27-3
Formula : C12H15NO2
M.W : 205.25
SMILES Code : O=C(OCC)NC1CC2=C(C=CC=C2)C1

Safety of [ 24446-27-3 ]

Application In Synthesis of [ 24446-27-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24446-27-3 ]

[ 24446-27-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 24446-27-3 ]
  • [ 2338-18-3 ]
  • 2
  • [ 541-41-3 ]
  • [ 2338-18-3 ]
  • [ 24446-27-3 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; triethylamine; In ice-water; dichloromethane; ethyl acetate; a) Ethyl indan-2-carbamate 200 ml of dichloromethane then 10 ml, i.e. 7.26 g (71.7 mmol) of triethylamine were added to 5 g (29.5 mmol) of <strong>[2338-18-3]2-aminoindan hydrochloride</strong>. The mixture was stirred for 30 min, then 3.4 ml, i.e. 3.84 g (35.4 mmol) of ethyl chloroformate were added dropwise. The mixture was stirred for 30 min, then ice-water and an excess of 1N hydrochloric acid were added. The precipitate was filtered, washed, dried and purified by chromatography on a silica gel column, eluted with an 80:20 mixture of dichloromethane/ethyl acetate. 4.25 g of amorphous solid were isolated. Melting point: 68-68.5 C.
 

Historical Records

Technical Information

Categories