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Chemical Structure| 24845-40-7 Chemical Structure| 24845-40-7

Structure of 24845-40-7

Chemical Structure| 24845-40-7

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Product Details of [ 24845-40-7 ]

CAS No. :24845-40-7
Formula : C15H14O2
M.W : 226.27
SMILES Code : O=C(C1=CC=CC=C1)CC2=CC=C(OC)C=C2
MDL No. :MFCD00096294
InChI Key :JABKESJVYSQBGF-UHFFFAOYSA-N
Pubchem ID :231092

Safety of [ 24845-40-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 24845-40-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24845-40-7 ]

[ 24845-40-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 24845-40-7 ]
  • [ 178686-24-3 ]
  • [ 57-13-6 ]
  • [ 1283117-23-6 ]
YieldReaction ConditionsOperation in experiment
10.8% With hydrogenchloride; In ethanol; water; for 96.0h;Reflux; [00164] To a solution of 2-(4-methoxyphenyl)-l-phenylethanone (100 mg, 0.44 mmol), <strong>[178686-24-3]3-ethoxy-4-hydroxy-5-nitrobenzaldehyde</strong> (93 mg, 0.44 mmol), and urea (60 mg, 1.32 mmol) in 20 mL of ethanol was added 0.2 mL of concentrated HCl, the mixture was stirred at reflux for 4 days. After the solvent was removed under reduced pressure, the residue was purified by thin layer chromatography (PE : EtOAc=l :2) to give Compound 19 (22 mg, yield 10.8%). 1H NMR (CD3OD 400 MHz): delta 7.55 (s, 1H), 7.20 (s, 5H), 7.12 (s, 1H), 6.73 (d, J = 8.4 Hz, 2H), 6.57 (d, J = 8.8 Hz, 2H), 5.25 (s, 1H), 4.05-4.00 (m, 2H), 3.61 (s, 3H), 1.35 (t, J = 6.8 Hz, 3H); MS (ESI): m/z 462.2 [M+l]+.
 

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