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Chemical Structure| 25519-81-7 Chemical Structure| 25519-81-7

Structure of 25519-81-7

Chemical Structure| 25519-81-7

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Product Details of [ 25519-81-7 ]

CAS No. :25519-81-7
Formula : C15H19NO3
M.W : 261.32
SMILES Code : COC1=CC=C(C=C1)C(=O)C1CCN(CC1)C(C)=O
MDL No. :MFCD19332058

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Application In Synthesis of [ 25519-81-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 25519-81-7 ]

[ 25519-81-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 25519-81-7 ]
  • [ 25519-82-8 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; water; In tetrahydrofuran; for 10h;Reflux; General procedure: To a solution of 1-(4-(2,3-dihydrobenzo[b][1,4] dioxine-6-carbonyl) piperidin-1-yl) ethanone 10a (3.13 g, 10 mmol) in 25 mL of THF was added 40 mL of 3 mol/L HCl. The reaction mixture was refluxed for 10 h. The solution was then concentrated in vacuo. The residue was recrystallized from MeOH/Ether to afford 11a (2.64 g, 93% yieid) as a white solid.
 

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