Home Cart 0 Sign in  

[ CAS No. 26103-48-0 ]

{[proInfo.proName]} ,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 26103-48-0
Chemical Structure| 26103-48-0
Structure of 26103-48-0 * Storage: {[proInfo.prStorage]}

Quality Control of [ 26103-48-0 ]

Related Doc. of [ 26103-48-0 ]

SDS
Alternatived Products of [ 26103-48-0 ]
Alternatived Products of [ 26103-48-0 ]

Product Details of [ 26103-48-0 ]

CAS No. :26103-48-0 MDL No. :MFCD00090297
Formula : C9H12N2O3S Boiling Point : 404°C at 760 mmHg
Linear Structure Formula :- InChI Key :-
M.W :228.27 g/mol Pubchem ID :-
Synonyms :

Safety of [ 26103-48-0 ]

Signal Word:Warning Class:
Precautionary Statements:P264-P270-P301+P312-P305+P351+P338-P330-P337+P313-P501 UN#:
Hazard Statements:H302-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 26103-48-0 ]

  • Downstream synthetic route of [ 26103-48-0 ]

[ 26103-48-0 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 110-91-8 ]
  • [ 16133-25-8 ]
  • [ 26103-48-0 ]
YieldReaction ConditionsOperation in experiment
In benzene at 0℃; for 0.5h; Yield given;
  • 2
  • [ 119-61-9 ]
  • [ 26103-48-0 ]
  • [ 88184-95-6 ]
YieldReaction ConditionsOperation in experiment
With n-butyllithium; diisopropylamine 1.) Et2O, -70 deg C, 1 h; 2.) Et2O, -70 deg C, 2 h; Yield given. Multistep reaction;
YieldReaction ConditionsOperation in experiment
81% 147 Anthracen-9-yl-[3-(morpholine-4-sulfonyl)-[1,4']bipiperidinyl-1'-yl]-methanone Trituration with methanol gave 4-(pyridine-3-sulfonyl)-morpholine as a pale yellow solid (14.29 g, 81%).
Pyridin-3-sulfonsaeure, PCl5, (Sulfochlorid), Amin.;
Pyridin-3-sulfonsaeure,Morpholin;
Sulfochlorid, Morpholin;

  • 4
  • [ 636-73-7 ]
  • [ 26103-48-0 ]
  • 5
  • [ 110-91-8 ]
  • [ 93056-12-3 ]
  • [ 26103-48-0 ]
YieldReaction ConditionsOperation in experiment
74% Stage #1: S-(3-pyridyl) benzothioate With trichloroisocyanuric acid; benzyltrimethylammonium chloride; sodium carbonate In water; acetonitrile at 0℃; for 0.333333h; Stage #2: morpholine In water; acetonitrile at 0 - 20℃; for 0.333333h; Typical procedure for the one-pot sulfonamide formation (Table 4, entry 10): To a stirred suspension of BnMe3NCl (142 mg, 0.76 mmol) in MeCN (2 ml) was added TCCA (57 mg, 0.25 mmol) and the mixture was left to stir for 30 min. The clear yellow solution obtained was added dropwise to a stirred 0 °C solution of the N1-tritylpyrazol-4-yl thiobenzoate (100 mg, 0.22 mmol) in MeCN (2 ml) over 2 min. To this mixture was added a 1 M solution of Na2CO3 (0.45 ml, 0.45 mmol) and the reaction was allowed to proceed at this temperature for 20 min. Morpholine (23 μl, 0.27 mmol) was added and mixture stirred for 20 min whilst warming to room temperature. At the end of the reaction, the mixture was partitioned between EtOAc (10 ml) and sat. Na2CO3 (10 ml). The EtOAc layer was washed with brine (10 ml), dried and concentrated in vacuo. The crude residue was purified by flash column chromatography, eluting with 0-20% EtOAc/heptane, yielding 86 mg (84% yield) of pure sulfonamide as a white solid.
  • 6
  • [ 1120-90-7 ]
  • [ 26103-48-0 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1.1: copper(l) iodide; 1,10-Phenanthroline; N-ethyl-N,N-diisopropylamine / toluene / 16 h / Reflux 2.1: trichloroisocyanuric acid; benzyltrimethylammonium chloride; sodium carbonate / water; acetonitrile / 0.33 h / 0 °C 2.2: 0.33 h / 0 - 20 °C
  • 7
  • [ 5765-65-1 ]
  • sodium pyridine-3-sulfinate [ No CAS ]
  • [ 26103-48-0 ]
YieldReaction ConditionsOperation in experiment
83% Stage #1: 4-(benzoyloxy)morpholine; sodium pyridine-3-sulfinate In 1,2-dichloro-ethane at 80℃; for 12h; Schlenk technique; Inert atmosphere; Stage #2: With copper(ll) bromide In 1,2-dichloro-ethane for 12h; Schlenk technique; Inert atmosphere;
  • 8
  • [ 36850-80-3 ]
  • [ 26103-48-0 ]
  • methyl 2-(3-(morpholinosulfonyl)pyridin-4-yl)acetate [ No CAS ]
YieldReaction ConditionsOperation in experiment
98% Stage #1: [(1-methoxyvinyl)oxy]trimethylsilane; 4-(pyridin-3-ylsulfonyl)morpholine With C26H17F6N2O6PS2 In acetonitrile at 20℃; for 20h; Inert atmosphere; Sealed tube; Stage #2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 0℃; for 3h;
Historical Records

Related Functional Groups of
[ 26103-48-0 ]

Sulfamides

Chemical Structure| 1352536-42-5

[ 1352536-42-5 ]

3-(Morpholinosulfonyl)pyridine-4-thiol

Similarity: 0.95

Chemical Structure| 627840-82-8

[ 627840-82-8 ]

5-(Morpholinosulfonyl)pyridin-2-amine

Similarity: 0.91

Chemical Structure| 1342018-01-2

[ 1342018-01-2 ]

3-(Morpholinosulfonyl)pyridin-4-amine

Similarity: 0.90

Chemical Structure| 889676-35-1

[ 889676-35-1 ]

4-((5-Bromopyridin-3-yl)sulfonyl)morpholine

Similarity: 0.89

Chemical Structure| 52480-33-8

[ 52480-33-8 ]

4-((6-Chloropyridin-3-yl)sulfonyl)morpholine

Similarity: 0.89

Related Parent Nucleus of
[ 26103-48-0 ]

Morpholines

Chemical Structure| 1352536-42-5

[ 1352536-42-5 ]

3-(Morpholinosulfonyl)pyridine-4-thiol

Similarity: 0.95

Chemical Structure| 627840-82-8

[ 627840-82-8 ]

5-(Morpholinosulfonyl)pyridin-2-amine

Similarity: 0.91

Chemical Structure| 1342018-01-2

[ 1342018-01-2 ]

3-(Morpholinosulfonyl)pyridin-4-amine

Similarity: 0.90

Chemical Structure| 889676-35-1

[ 889676-35-1 ]

4-((5-Bromopyridin-3-yl)sulfonyl)morpholine

Similarity: 0.89

Chemical Structure| 52480-33-8

[ 52480-33-8 ]

4-((6-Chloropyridin-3-yl)sulfonyl)morpholine

Similarity: 0.89

Pyridines

Chemical Structure| 1352536-42-5

[ 1352536-42-5 ]

3-(Morpholinosulfonyl)pyridine-4-thiol

Similarity: 0.95

Chemical Structure| 627840-82-8

[ 627840-82-8 ]

5-(Morpholinosulfonyl)pyridin-2-amine

Similarity: 0.91

Chemical Structure| 1342018-01-2

[ 1342018-01-2 ]

3-(Morpholinosulfonyl)pyridin-4-amine

Similarity: 0.90

Chemical Structure| 889676-35-1

[ 889676-35-1 ]

4-((5-Bromopyridin-3-yl)sulfonyl)morpholine

Similarity: 0.89

Chemical Structure| 52480-33-8

[ 52480-33-8 ]

4-((6-Chloropyridin-3-yl)sulfonyl)morpholine

Similarity: 0.89