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Chemical Structure| 28547-08-2 Chemical Structure| 28547-08-2

Structure of 28547-08-2

Chemical Structure| 28547-08-2

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Product Details of [ 28547-08-2 ]

CAS No. :28547-08-2
Formula : C9H8ClNO3
M.W : 213.62
SMILES Code : O=C(O)C1=CC=CC(NC(CCl)=O)=C1
MDL No. :MFCD02379857

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Application In Synthesis of [ 28547-08-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 28547-08-2 ]

[ 28547-08-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 28547-08-2 ]
  • [ 55690-60-3 ]
  • 3-(2-(5-methoxybenzo[d]thiazol-2-ylthio)acetamido)benzoic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
63% With potassium carbonate; In acetone; for 6h;Reflux; General procedure: A mixture of substituted 3-(2-chloroacetamido)benzoicacids (2a or 2b) (1 mmol), substituted 2-mercapto benzothiazoles(3a-j) (1 mmol) and K2CO3 (0.207g, 1.5 mmol) wasrefluxed in dried acetone (20 ml) for 5-6 h. Excess of solventin reaction mixture was evaporated at room temperature, andthe concentrate was diluted with water (about 200 ml). Theproduct precipitated out on acidification with dilute hydrochloricacid was filtered and thoroughly washed with coldwater to yield the title compounds [19-23].
 

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