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Chemical Structure| 288105-04-4 Chemical Structure| 288105-04-4

Structure of 288105-04-4

Chemical Structure| 288105-04-4

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Product Details of [ 288105-04-4 ]

CAS No. :288105-04-4
Formula : C20H17BO2
M.W : 300.16
SMILES Code : OB(C1=CC=C(/C=C(C2=CC=CC=C2)\C3=CC=CC=C3)C=C1)O
MDL No. :MFCD12911571

Safety of [ 288105-04-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 288105-04-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 288105-04-4 ]

[ 288105-04-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 66127-01-3 ]
  • [ 288105-04-4 ]
  • 3-(4-(2,2-diphenylvinyl)phenyl)-1,10-phenanthroline [ No CAS ]
YieldReaction ConditionsOperation in experiment
69% Under nitrogen atmosphere, <strong>[66127-01-3]3-bromophenanthroline</strong> (0.10 g, 0.40 mmol), 4-(2,2-diphenylvinyl)phenyl]boronic acid (0.14 g, 0.48mmol), tetrakis(triphenylphosphine)palladium, 20mL of tetrahydrofuran was added 100mL three-necked round bottom flask was stirred at room temperature for 10min, the reaction system was added 4mL aqueous solution of sodium carbonate (2M) and reacted at 70 C for 24 h. After the reaction was completed, most of the tetrahydrofuran was distilled off, extracted with methylene chloride, washed with water, dried over anhydrous sodium sulfate, concentrated and subjected to column chromatography (SiO2, eluent: dichloromethane / methanol = 19: 1) afforded 0.12 g of the DP product in 69.0% yield.
 

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