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[ CAS No. 29064-82-2 ] {[proInfo.proName]}

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Chemical Structure| 29064-82-2
Chemical Structure| 29064-82-2
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Product Details of [ 29064-82-2 ]

CAS No. :29064-82-2 MDL No. :MFCD08275122
Formula : C7H3BrClNS Boiling Point : -
Linear Structure Formula :- InChI Key :FXIKIVFBAQCMRY-UHFFFAOYSA-N
M.W : 248.53 Pubchem ID :18450773
Synonyms :

Safety of [ 29064-82-2 ]

Signal Word:Warning Class:
Precautionary Statements:P280-P305+P351+P338 UN#:
Hazard Statements:H317-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 29064-82-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29064-82-2 ]

[ 29064-82-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 29064-82-2 ]
  • [ 17413-10-4 ]
  • (3-Bromo-thieno[3,2-c]pyridin-4-yl)-(2,3-dihydro-benzo[1,4]dioxin-6-ylmethyl)-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
77% With triethylamine; In 1-methyl-pyrrolidin-2-one; at 220℃; for 2h;Microwave; A stirred mixture of 3-bromo-4-chloro-thieno[3,2-c]pyridine (200 mg, 0.80 mmol), 2,3-dihydro-1,4-benzodioxin-6-yl-methylaminebenzylamine (266 mg, 1.61 mmol), and triethylamine (112 mul, 0.80 mmol) in NMP (2 ml) was heated in a Biotage microwave reactor for 2 h at 220 C. At which point the reaction was allowed to cool to room temperature and partitioned between EtOAc (10 ml) and distilled water (10 ml). The organic layer was separated and washed with additional portions of distilled water (2×10 ml), dried (MgSO4), filtered and the solvent removed in vacuo. The crude residue was then subjected to flash column chromatography (eluent petroleum spirit 40-60 C.:EtOAc, 3:1, Rf 0.6). This afforded the title compound as a yellow solid (233 mg, 77%).
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