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Chemical Structure| 29193-63-3 Chemical Structure| 29193-63-3

Structure of 29193-63-3

Chemical Structure| 29193-63-3

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Product Details of [ 29193-63-3 ]

CAS No. :29193-63-3
Formula : C10H11ClO2S
M.W : 230.71
SMILES Code : O=C(O)CCCSC1=CC=C(Cl)C=C1
MDL No. :MFCD00460787

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Application In Synthesis of [ 29193-63-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 29193-63-3 ]

[ 29193-63-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 80-65-9 ]
  • [ 29193-63-3 ]
  • 4-((4-chlorophenyl)thio)-N-(2-oxooxazolidin-3-yl)butanamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
63.5% General procedure: Following the addition of 4-(4-fluorophenoxy) butyric acid (0.71 g, 3.6 mmol) to 20 mL ofdichloromethane in a 50 mL three-necked round-bottom flask, thesolution was agitated until dissolution. Subsequently, EDCI (0.85 g,4.44 mmol) HOBt (0.6 g, 4.44 mmol) and triethylamine (0.84 g,9.25 mmol) were added in turn at 0 C. Stirring in an ice bath for 1 h,<strong>[80-65-9]3-amino-2-oxazolidinone</strong> (0.37 g, 3.6 mmol) was added again. Thesolutionwas brought to 25 C and stirred overnight. Following TLC,the product was filtered by vacuum and dried under rotary evaporation.The product was a white solid weighing 0.51 g with a yieldof 50.2%.
 

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