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Chemical Structure| 3010-80-8 Chemical Structure| 3010-80-8

Structure of 3010-80-8

Chemical Structure| 3010-80-8

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Product Details of [ 3010-80-8 ]

CAS No. :3010-80-8
Formula : C19H13Cl3O
M.W : 363.67
SMILES Code : OC(C1=CC=C(Cl)C=C1)(C2=CC=C(Cl)C=C2)C3=CC=C(Cl)C=C3
MDL No. :MFCD00051795

Safety of [ 3010-80-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 3010-80-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 3010-80-8 ]

[ 3010-80-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 288-32-4 ]
  • [ 3010-80-8 ]
  • [ 15469-97-3 ]
  • [ 37594-47-1 ]
YieldReaction ConditionsOperation in experiment
With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; EXAMPLE 4 N-([4,4',4"]-Trichlorotrityl)imidazole (7) To a stirred solution of tris(4-chlorophenyl)methanol (0.36 g, 1.0 mmol) and imidazole (0.20 g, 2.9 mmol) in 2 mL of CH2 Cl2 under N2 at RT was added 0.40 mL (2.0 mmol) of trimethylsilyl triflate. After 1 h, the crude product was isolated as described for (2) and purified by flash chromatography (10percent EtOAc-hexanes.(R).EtOAc) to give 0.25 g of a semisolid. This material was triturated with 5percent Et2 O-hexanes to give 0.20 g of (7) as a white solid, m.p. 153°-155° C. IR (KBr) 1490, 1399, 1217, 1097, 1080, 1013, 815 cm-1. NMR (CDCl3): d 6.77, 7.10, 7.41 (each s, 1H, imidazole CH); 7.04 (dt, 6H); 7.33 (dt, 6H). Anal. Calc'd (C22 H15 N2 Cl3): C, 63.86; H, 3.65; N, 6.77. Found: 63.96; 3.95; 6.70.
 

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