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Structure of 30557-06-3

Chemical Structure| 30557-06-3

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Product Details of [ 30557-06-3 ]

CAS No. :30557-06-3
Formula : C10H11NO2
M.W : 177.20
SMILES Code : O=C1NC2=C(C(OC)=CC=C2)CC1
MDL No. :MFCD09955248
InChI Key :IAAVILGMVWQJDL-UHFFFAOYSA-N
Pubchem ID :12947118

Safety of [ 30557-06-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 30557-06-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 30557-06-3 ]

[ 30557-06-3 ] Synthesis Path-Downstream   1~2

  • 1
  • C11H13NO4S [ No CAS ]
  • [ 30557-06-3 ]
  • [ 129075-49-6 ]
  • 2
  • [ 30557-06-3 ]
  • [ 160893-04-9 ]
YieldReaction ConditionsOperation in experiment
91% With sodium persulfate; iron(III) chloride hexahydrate; In water; acetonitrile; at 80℃; Compound I-3 (177 mg, 1 mmol), ferric trichloride hexahydrate (2.7 mg, 0.01 mmol) and sodium peroxodisulfate (286 mg, 1.2 mmol) were added to a reaction flask with a reflux condenser, and acetonitrile (5 mL) was added. ) And water (5 mL) and stir well at room temperature. The mixture was stirred with heating at 80 C for 2-3 hours until the reaction was completed. The reaction mixture was concentrated by heating to remove most of the acetonitrile, and then slowly cooled to room temperature, a white solid was slowly precipitated, and dried by filtration to obtain 160 mg of the product II-3 as an off-white solid, with a yield of 91%.
 

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