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[ CAS No. 33375-06-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
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Chemical Structure| 33375-06-3
Chemical Structure| 33375-06-3
Structure of 33375-06-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 33375-06-3 ]

CAS No. :33375-06-3 MDL No. :MFCD00063015
Formula : C9H9NO Boiling Point : -
Linear Structure Formula :- InChI Key :JJSCUXAFAJEQGB-MRVPVSSYSA-N
M.W :147.17 Pubchem ID :7018262
Synonyms :

Safety of [ 33375-06-3 ]

Signal Word:Danger Class:6.1
Precautionary Statements:P233-P260-P261-P264-P270-P271-P280-P301+P310-P302+P352-P304-P304+P340-P305+P351+P338-P312-P321-P322-P330-P332+P313-P337+P313-P340-P361-P362-P363-P403-P403+P233-P405-P501 UN#:2206
Hazard Statements:H301-H311-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 33375-06-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 33375-06-3 ]

[ 33375-06-3 ] Synthesis Path-Downstream   1~12

  • 1
  • [ 33375-06-3 ]
  • [ 6327-59-9 ]
  • (S)-2-[3-((R)-1-Phenyl-ethyl)-ureido]-succinic acid dibenzyl ester [ No CAS ]
  • 2
  • [ 33375-06-3 ]
  • [ 3728-20-9 ]
  • [ 145401-85-0 ]
  • 3
  • [ 1487-49-6 ]
  • [ 33375-06-3 ]
  • (R)-3-((R)-1-Phenyl-ethylcarbamoyloxy)-butyric acid methyl ester [ No CAS ]
  • (S)-3-((R)-1-Phenyl-ethylcarbamoyloxy)-butyric acid methyl ester [ No CAS ]
YieldReaction ConditionsOperation in experiment
In toluene 1.) 2 h, 100 deg C, MeOH, 2 h, reflux;
  • 4
  • [ 33375-06-3 ]
  • [ 54143-55-4 ]
  • N-<N-<(R)-1-Phenylethylcarbamoyl>-(S)-2-piperidylmethyl>-2,5-bis(2,2,2-trifluorethoxy)benzamid [ No CAS ]
  • N-<N-<(R)-1-Phenylethylcarbamoyl>-(R)-2-piperidylmethyl>-2,5-bis(2,2,2-trifluorethoxy)benzamid [ No CAS ]
YieldReaction ConditionsOperation in experiment
In dichloromethane at 20℃; for 0.333333h;
  • 5
  • [ 33375-06-3 ]
  • [ 109-07-9 ]
  • 1,4-bis(R-1-phenylethylcarbamoyl)-RS-2-methylpiperazine [ No CAS ]
  • 6
  • [ 33375-06-3 ]
  • [ 75449-26-2 ]
  • 3'-<3-(α-Methylbenzyl)ureido>-2,2'-bipyridin-3-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
87% In toluene at 80℃; for 2h;
  • 7
  • [ 33375-06-3 ]
  • [ 6530-09-2 ]
  • 1-(S)-1-Aza-bicyclo[2.2.2]oct-3-yl-3-((R)-1-phenyl-ethyl)-urea [ No CAS ]
  • 1-(R)-1-Aza-bicyclo[2.2.2]oct-3-yl-3-((R)-1-phenyl-ethyl)-urea [ No CAS ]
  • 8
  • [ 33375-06-3 ]
  • [ 85958-57-2 ]
  • (R)-N5-(tert.-butoxy-carbonyl)-N2-(9-fluorenylmethoxycarbonyl)-ornithine [ No CAS ]
  • (R)-2-(2-Chloro-4-fluoro-benzenesulfonylamino)-5-[3-((R)-1-phenyl-ethyl)-ureido]-pentanoic acid hydroxyamide [ No CAS ]
  • 9
  • [ 33375-06-3 ]
  • [ 301225-58-1 ]
  • 4-[3-(1-phenyl-ethyl)-1-propyl-ureido]-piperidine-1-carboxylic acid <i>tert</i>-butyl ester [ No CAS ]
  • 10
  • [ 2524-67-6 ]
  • [ 555-57-7 ]
  • [ 33375-06-3 ]
  • C36H29IN2O6 [ No CAS ]
  • C63H58N6O7 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Stage #1: Pargyline; C36H29IN2O6 With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In N,N-dimethyl-formamide at 20℃; for 72h; Stage #2: 4-morpholino-4-yl-phenylamine With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide at 20℃; for 24h; Stage #3: (1R)-1-phenylethyl isocyanate With dmap; triethylamine In tetrahydrofuran at 20℃; for 48h;
  • 11
  • [ 30235-28-0 ]
  • [ 33375-06-3 ]
  • [ 1342276-85-0 ]
YieldReaction ConditionsOperation in experiment
54% In 1-methyl-pyrrolidin-2-one; at 150℃; for 0.333333h; COMPOUND lah(R)-l-(l-Phenylethyl)-3-(4-(pyridin-4-yl)thiazol-2-yl)urea. This was prepared from 3a (0.126 g, 0.711 mmol) and (R)-(+)-alpha-methylbenzyl isocyanate (0.209 g, 1.42 mmol) in the same manner as described for laa. Chromatography on silica gel performed twice using the FlashMaster 3 purification station, afforded lah as a white solid (0.125 g, 0.385 mmol, 54%). 1H NMR (400 MHz, DMSO-d6) delta 10.51 (s, 1H), 8.56 (d, J= 5.8 Hz, 2H), 7.80 (s, 1H), 7.76 (d, J= 6.0 Hz, 2H), 7.36-7.31 (m, 4H), 7.26-7.24 (m, 1H), 7.02 (d, J = 7.7 Hz, 1H), 4.84 (quint, J= 7.3 Hz, 1H), 1.40 (d, J= 6.9 Hz, 6H); 13C NMR (400 MHz, DMSO-d6) delta 160.80, 153.72, 150.84, 146.77, 145.01, 141.64, 129.14, 127.61, 126.47, 120.48, 1 1 1.71 , 49.71 , 23.54; HPLC purity 99.22% {tR = 7.907 min, Flow lml/min,[(CH3CN/(0.1% TFA in H2O):30/70] ; purity 99.51% {tR = 8.653 min, Flow lml/min, [(MeOH/(0.1% TFA in H2O):50/50] ; HRMS (ESI +ve) m z calculated for C17H17N4OS (M + H)+ 3251 1 17, found 325.1 1 16.The enantiomeric excess was determined by HPLC using a Chiralcel OJ column[(/so-propanol/Hexane:50/50), Flow lml/min], tRi = 9.067 min, Area %> 0.404 (minor), 14.300 min, Area % 98.378 (major).
  • 12
  • [ 7341-24-4 ]
  • [ 33375-06-3 ]
  • [ 1404592-03-5 ]
YieldReaction ConditionsOperation in experiment
at 20℃; for 1.5h;
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