Home Cart Sign in  
Chemical Structure| 342613-84-7 Chemical Structure| 342613-84-7

Structure of 342613-84-7

Chemical Structure| 342613-84-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 342613-84-7 ]

CAS No. :342613-84-7
Formula : C13H10N2
M.W : 194.23
SMILES Code : N#CC1=CC=CC=C1C2=CC=CC(N)=C2

Safety of [ 342613-84-7 ]

Application In Synthesis of [ 342613-84-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 342613-84-7 ]

[ 342613-84-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 342613-84-7 ]
  • [ 52854-14-5 ]
  • [ 689298-05-3 ]
YieldReaction ConditionsOperation in experiment
38% With triethylamine; In dimethyl sulfoxide; at 90℃; for 18.0h; The above product (3.50 g, 18.5 mmol) and 3'-aminobiphenyl-2-carbonitrile (prepared according to the procedure described in WO 02/38568) (3.23 g, 16.6 mmol) were dissolved in triethylamine (9. 32 g, 92.3 mmol) and dimethylsulfoxide (10 ml) and heated at 90C for 18 h. The mixture was allowed to cool to ambient temperature then poured onto water (150 ml) and extracted with ethyl acetate (2 x 300 ml). The organic fractions were combined, washed with water (3 x 75 ml) and brine (50 ml), dried over anhydrous sodium sulfate, filtered and evaporated to give a brown solid. The brown solid was triturated with diethyl ether (50 ml), filtered, washed with diethyl ether (2 x 10 ml) and left to air dry, which gave 3'- (1-methyl-5-nitro-6-oxo-1, 6-DIHYDROPYRIMIDIN-4-YLAMINO) biphenyl-2-carbonitrile (2.24 g, 38%) as a yellow solid
 

Historical Records

Technical Information

Categories