Home Cart Sign in  
Chemical Structure| 347-91-1 Chemical Structure| 347-91-1

Structure of 347-91-1

Chemical Structure| 347-91-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 347-91-1 ]

CAS No. :347-91-1
Formula : C14H11FO
M.W : 214.24
SMILES Code : FC1=CC=C(CC(C2=CC=CC=C2)=O)C=C1
MDL No. :MFCD02260684
InChI Key :CWYRBOMWOQXYFZ-UHFFFAOYSA-N
Pubchem ID :236329

Safety of [ 347-91-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 347-91-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 347-91-1 ]

[ 347-91-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 71-43-2 ]
  • [ 459-04-1 ]
  • [ 347-91-1 ]
YieldReaction ConditionsOperation in experiment
97% aluminum (III) chloride; at 25 - 50℃; for 8.5h; 2- (4-Fluoro-phenyl)-1-phenyl-ethanone To a solution of benzene (182 mL) at 0 C was added AIC13 (46.4 g, 348 mmol). A portion of 4-fluorophenyl acetyl chloride (50.0 g, 290 mmol) was then added drop- wise over 30 min. Once the addition was complete, the reaction was allowed to warm to 25 C and then heated to 50 C for 8 hr. Subsequently, the reaction mixture was cooled to 25 C and poured onto ice (400 g). To the resulting suspension in ice was added 1.0 N HCI (50 mL). The organic layer was separated and washed with 10% HCI, saturated NaHC03 and brine. The organic layer was then dried and concentrated to afford a solid that was washed twice with hexane (200 mL) and then dried under vacuum to afford 2- (4-fluoro-phenyl)-1-phenyl-ethanone (59.90 g, 97%): MS (APCI+) : Sz 215.0 (M+H); H-NMR (CDCI3) o ?. 82 (d, 2 H), 7.54-7. 41 (m, 3 H), 7.22-7. 17 (m, 2 H), 7.00-6. 96 (m, 2 H), 4.23 (s, 3 H).
  • 2
  • [ 395-21-1 ]
  • [ 347-84-2 ]
  • [ 347-91-1 ]
 

Historical Records

Technical Information

Categories