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CAS No. : | 34837-88-2 | MDL No. : | MFCD09754963 |
Formula : | C10H11NO5 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | HAFCSCBORMDMFL-UHFFFAOYSA-N |
M.W : | 225.20 | Pubchem ID : | 13846354 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
96% | at 20℃; | N-((4-chloro-2-methylphenyl)(phenyl)methyl)-2-methyl-2-(2-(2-methylpyridin-3- yl)benzo[a) methyl 2-(4-methoxy-3-nitrophenyl)acetateTo a solution of methyl 2-(4-hydroxy-3-nitrophenyl)acetate (4.87 g, 23.1 mmol) at rt was added K2CO3 (8 g, 58 mmol), followed by slow addition of CH3I (6.6 g, 46.5 mmol). The reaction mixture was stirred at rt overnight. The reaction mixture was then poured into ice-water (100 mL) and extracted with CH2CI2 (3 x 300 mL). The combined organic layers were washed with brine, dried over Na2S04, filtered, and concentrated to afford the title compound (5 g, 96percent) as a yellow solid. LCMS-P1 : 226.0 [M+H]+; Rt: 1.438 min. |
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