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Chemical Structure| 35028-14-9 Chemical Structure| 35028-14-9

Structure of 35028-14-9

Chemical Structure| 35028-14-9

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Product Details of [ 35028-14-9 ]

CAS No. :35028-14-9
Formula : C11H14O
M.W : 162.23
SMILES Code : CCC(C1=CC=CC(C)=C1C)=O
MDL No. :MFCD11617671
Boiling Point : No data available

Safety of [ 35028-14-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 35028-14-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 35028-14-9 ]

[ 35028-14-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 50-00-0 ]
  • [ 25150-61-2 ]
  • [ 35028-14-9 ]
  • 1-(2,3-Dimethyl-phenyl)-2-methyl-3-pyrrolidin-1-yl-propan-1-one [ No CAS ]
  • 2
  • [ 25150-61-2 ]
  • [ 35028-14-9 ]
  • 2-methyl-1-(2,3-dimethylphenyl)-3-pyrrolidino-1-propanone hydrochloride [ No CAS ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; paraformaldehyde; In water; EXAMPLE 4 2-Methyl-1-(2,3-dimethylphenyl)-3-pyrrolidino-1-propanone (Compd. No. 1-13) hydrochloride. A mixture of 1-(2,3-dimethylphenyl)-1-propanone (11.2 g), paraformaldehyde (2.70 g), pyrrolidine-hydrochloride (9.7g), and hydrochloric acid (0.5 ml) in isopropyl alcohol (15 ml) was refluxed for 8.5 hours. The reaction mixture was evaporated in vacuo to give the residue. The residue was dissolved in water and then washed with ethyl acetate. The aqueous layer was extracted with dichloromethane and then dried over anhydrous magnesium sulfate. The mixture was filtered and then the filtrate was evaporated in vacuo to give the residue. The residue was recrystallized from CH2 Cl2 - AcOEt to give 2-methyl-1-(2,3-dimethylphenyl)-3-pyrrolidino-1-propanone hydrochloride (13.1 g, Y: 64.7%) as colorless prisms, m.p. 149-151 C. IR ν (the free base)maxneat: 1690 cm-1 STR323 Mass (the free base) m/z (relative intensity): 245 (M+, 0.0097), 174 (30.5), 159 (40.2), 133 (76.3), 105 84 (100).
 

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