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Chemical Structure| 35444-93-0 Chemical Structure| 35444-93-0

Structure of 35444-93-0

Chemical Structure| 35444-93-0

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Product Details of [ 35444-93-0 ]

CAS No. :35444-93-0
Formula : C13H11I
M.W : 294.13
SMILES Code : IC1=CC=CC=C1CC2=CC=CC=C2
MDL No. :MFCD00270110

Safety of [ 35444-93-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 35444-93-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 35444-93-0 ]

[ 35444-93-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 35444-93-0 ]
  • [ 100-47-0 ]
  • [ 3469-20-3 ]
YieldReaction ConditionsOperation in experiment
72% With potassium tert-butylate; copper(II) sulfate; In octane; tert-butyl alcohol;Schlenk technique; Inert atmosphere; Sealed tube; Adding 0.02 equivalents of anhydrous copper sulfate and 4.0 equivalents of potassium t-butoxide to a 25 mL Schlenk reaction tube, drying in vacuum for 15 minutes, and adding 1.5 mL of n-octane and 1 mL of t-butanol, 5.0 equivalents of benzonitrile in an argon atmosphere, 2 mmol of 1-benzyl-2-iodobenzene, in the reaction tube after adding polytetrafluoroethylene stopper was placed into an oil bath of the reaction 60 °C for 20 hours. After the reaction is completed, the solvent is removed by filtration, and the residue is purified by column chromatography, eluting with petroleum ether / methylene chloride / ethyl acetate (v: v: v = 20:10:1) to give a colorless liquid, 2,3-diphenyl indole. The yield was 72percent
 

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