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Chemical Structure| 3708-04-1 Chemical Structure| 3708-04-1

Structure of 3708-04-1

Chemical Structure| 3708-04-1

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Product Details of [ 3708-04-1 ]

CAS No. :3708-04-1
Formula : C9H10O3S
M.W : 198.24
SMILES Code : O=S(CC(C1=CC=CC=C1)=O)(C)=O
MDL No. :MFCD00025078
InChI Key :CAUSPZIZBLGLKW-UHFFFAOYSA-N
Pubchem ID :19457

Safety of [ 3708-04-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H318
Precautionary Statements:P264-P270-P280-P301+P312-P305+P351+P338-P310-P330-P501
Class:8
UN#:1759
Packing Group:

Application In Synthesis of [ 3708-04-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 3708-04-1 ]

[ 3708-04-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 103646-82-8 ]
  • [ 3708-04-1 ]
  • 5-methanesulfonyl-1-(4-methylphenyl)-6-phenyl-1H-pyrazolo[3,4-b]pyridin-4-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
77% General procedure: (General method). Amixture of the appropriate aminonitrile 1 (3.0 mmol) and1,3-dicarbonyl compound (3.0 mmol) in anhydrous toluene(12 ml) was refluxed for 1 h in a flask equipped with aDean?Stark trap. Tin(IV) chloride (3.0 g, 11.5 mmol) wasadded to the reaction mixture, and refluxing was continuedfor additional 5?6 h. A resinous precipitate was formed,andthe colorless toluene layer was decanted. The residualsolvent was removed on a rotary evaporator, the obtainedglassy solids were dissolved in boiling dioxane, cooled, thenpoured into a solution of Na23 (4.0 g) in water (70 ml).The precipitate that formed was filtered off, washed withwater, dried, and recrystallized from a 5:1 mixture of2-PrOH?DMF.
 

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