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Chemical Structure| 388091-63-2 Chemical Structure| 388091-63-2

Structure of 388091-63-2

Chemical Structure| 388091-63-2

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Product Details of [ 388091-63-2 ]

CAS No. :388091-63-2
Formula : C15H13ClO
M.W : 244.72
SMILES Code : O=C(C1=CC=CC(Cl)=C1)CCC2=CC=CC=C2
MDL No. :MFCD03842927

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Application In Synthesis of [ 388091-63-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 388091-63-2 ]

[ 388091-63-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 120121-01-9 ]
  • [ 388091-63-2 ]
  • 2
  • [ 120121-01-9 ]
  • [ 100-51-6 ]
  • [ 388091-63-2 ]
YieldReaction ConditionsOperation in experiment
83% A solution of 1- (3-chlorophenyl) ethanol cat(Ir) (5.3 mg, 0.01 mmol, 1 mol%) and tert-amyl alcohol (1 mL) were successively added to a 5 mL round bottom flask. The reaction mixture was refluxed in air for 6 hours and then cooled to room temperature. Then, cesium carbonate (33 mg, 0.1 mmol, 0.1 equiv.) And benzyl alcohol (119 mg, 1.1 mmol) were added, refluxed in air for 6 hours, and then cooled to room temperature. The solvent was removed by rotary evaporation and then the title compound was purified by column chromatography (developing solvent: petroleum ether / ethyl acetate) in 83%
 

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