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Chemical Structure| 40748-71-8 Chemical Structure| 40748-71-8

Structure of 40748-71-8

Chemical Structure| 40748-71-8

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Product Details of [ 40748-71-8 ]

CAS No. :40748-71-8
Formula : C14H19NO
M.W : 217.31
SMILES Code : O=C1C(CC)CN(CC2=CC=CC=C2)CC1
MDL No. :MFCD07394314

Safety of [ 40748-71-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H319
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 40748-71-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 40748-71-8 ]

[ 40748-71-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 57611-47-9 ]
  • [ 40748-71-8 ]
  • 2
  • [ 40748-71-8 ]
  • [ 14150-94-8 ]
  • 6-benzyl-8-ethyl-3-nitro-5,6,7,8-tetrahydro-1,6-naphthyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
With ammonia; In methanol; at 100℃;Inert atmosphere; Into a 1000 mL pressure tank reactor purged and maintained with an inert atmosphere of nitrogen was placed 1-benzyl-3-ethylpiperidin-4-one (28 g, 129 mmol), <strong>[14150-94-8]1-methyl-3,5-dinitro-1,2-dihydropyridin-2-one</strong> (25.7 g, 129 mmol) and 7M ammonia in methanol (500 mL). The resulting solution was stirred overnight at 100C in an oil bath. The cooled reaction was concentrated to yield crude title compound (45 g, quant crude yield) as a solid.
 

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