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Chemical Structure| 41219-16-3 Chemical Structure| 41219-16-3

Structure of 41219-16-3

Chemical Structure| 41219-16-3

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Product Details of [ 41219-16-3 ]

CAS No. :41219-16-3
Formula : C10H15NO3
M.W : 197.23
SMILES Code : NCC1=CC=C(OC)C(OC)=C1OC
MDL No. :MFCD01310841

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Application In Synthesis of [ 41219-16-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 41219-16-3 ]

[ 41219-16-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 41219-16-3 ]
  • [ 112811-71-9 ]
  • C26H29FN2O7 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In dimethyl sulfoxide; N,N-dimethyl-formamide; at 120℃; for 6h; A three-necked flask was charged with 100 g of ethyl l-cyclopropyl-6,7-difluoro-8-methoxy-1,4-dihydro-4-oxo-3-quinolinecarboxylate,Then, a mixed solvent of 600 mL of DMF: DMSO = 1: 1 was added thereto and stirred. 62.2 mL of 2,3,4-trimethoxybenzylamine was added,Heated to 120 C for 6h, cooled, the reaction was poured into lmol / L dilute hydrochloric acid, stirred, added 500mLEA extraction, the organic layer was separated, the aqueous phase was extracted with EA300mLX2,The combined organic layers were dried and evaporated to dryness to give 92.3 g of the yellow product which was used in the next step without further purification.
 

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